Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
The celebrated M. de Jussieu having viewed the whole himself, in a
journey he made to this mine, furnished us with this description of the
work.
PROCESS II.
_To give Mercury, by the action of Fire, the appearance of a Metalline
Calx._
Put Mercury into several little glass matrasses with long and narrow
necks. Stop the matrasses with a little paper, to prevent any dirt from
falling into them. Set them all in one sand-bath, so that they may
be surrounded with sand as high as two thirds of their length. Apply
the strongest degree of heat that Mercury can bear without subliming:
continue this heat without interruption, till all the Mercury be turned
to a red powder. The operation lasts about three months.
_OBSERVATIONS._
Mercury treated according to the process here delivered hath all
the appearance of a metalline calx, but it hath no more: for, if it
be exposed to a pretty strong degree of fire, it sublimes, and is
wholly reduced to running Mercury, without the addition of any other
inflammable matter; which proves that during this long calcination it
lost none of its phlogiston.
The volatile nature of Mercury, which permits it not to bear a heat
of any strength without subliming, prevents our examining all the
effects that fire is capable of producing on it. Yet there is reason
to believe that, as this metallic substance resembles the perfect
metals in its weight, its splendour, and a brilliancy which resists all
the impressions of the air without alteration, it would like them be
unchangeable by the greatest force of fire, if it were fixed enough to
bear it.
In order to give Mercury the form of a metalline calx, it must
necessarily be exposed for about three months together, to the utmost
heat it can bear without subliming, as is above directed. Boerhaave
kept it digesting in a less heat for fifteen years successively, both
in open and in close vessels, without observing it to suffer the least
change; except that there was formed upon its surface a small quantity
of a black powder, which was reduced to running Mercury by trituration
alone.
Mercury thus converted to a red powder is known in chymistry and
medicine by the name of _Mercury precipitated per se_: a title proper
enough, as it is actually reduced to the form of a precipitate, and
that without any additament; but very improper on the other hand,
considering, that in reality this Mercury is not a precipitate, as not
having been separated from any menstruum in which it was dissolved.
PROCESS III.
_To dissolve Mercury in the Vitriolic Acid. Turbith Mineral._
Put Mercury into a glass retort, and pour on it thrice its weight of
good Oil of Vitriol. Set the retort in a sand-bath; fit on a recipient;
warm the bath by degrees till the liquor just simmer. With this heat
the Mercury will begin to dissolve. Continue the fire in this degree
till all the Mercury be dissolved.
_OBSERVATIONS._
Public-domain text, read in full here on John Shaqi.
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