Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
The specific gravity of beer is determined by first removing the excess
of carbonic acid by repeatedly agitating the sample in a capacious
glass flask, or by pouring it from one beaker into another several
times, and then filling a specific gravity bottle with the liquid and
allowing it to stand at rest until all air or gas bubbles have escaped;
the weight of the bottle and its contents is now taken at 15°. In order
to determine the proportion of alcohol present, 100 c.c. of the beer
are introduced in a suitable flask which is connected with a Liebig’s
condenser and subjected to distillation until about one-half of the
quantity taken has passed over. The distillate is then made up to its
original volume by the addition of water, and its density ascertained
by means of the specific gravity bottle, from which the percentage of
alcohol present (by weight and by volume) is readily obtained upon
referring to the alcoholometric table on p. 144. The frothing of beer
and the volatilisation of the free acids present are best obviated by
the addition of a little tannic acid and baryta-water to the sample
before the distillation. An indirect method for the determination
of alcohol in beer is also frequently employed. It is accomplished
by first ascertaining the density of the liquor, next removing the
alcohol present by evaporation over the water-bath, subsequently adding
sufficient water to restore the original volume and again taking
the specific gravity of the product. The density of spirit of equal
strength to the beer taken (X) is obtained by the formula, D/D´ = X,
in which D is the original gravity of the sample, and D´ the gravity
of the de-alcoholised liquor when made up to its first volume. The
following table (see p. 144) from ‘Watts’ Dictionary of Chemistry’
gives the percentages of alcohol by volume and weight, corresponding to
different densities at 15°.
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