Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
_Maumené’s test._--This test is founded upon the fact that the
elevation of temperature caused by mixing olive oil with strong
sulphuric acid is considerably less than that produced with the oils
commonly employed as its adulterants. With these latter an evolution
of sulphurous acid generally takes place, which is not the case with
pure olive oil. The best method of procedure is as follows:--10 c.c. of
sulphuric acid (sp. gr. 1·844) are gradually added to 50 grammes of the
sample, the mixture being constantly stirred with a small thermometer,
and observations made of the maximum increase of temperature produced,
as well as of the evolution of gas. When treated in this manner,
genuine olive oil causes an elevation of about 42°; that given by
various other oils, often added to it, ranges from 52° to 103°, and
it is frequently possible to recognise their presence in admixtures
by the high temperature produced. The following are the increases
of temperature observed by L. Archbutt:--olive, 41-45; rape, 55-64;
arachis, 47-60; sesamé, 65; cotton-seed (crude) 70; (refined), 75-76;
poppy-seed, 86-88; menhaden, 123-128. In the Paris Municipal Laboratory
an acid of 1·834 sp. gr. is used, and the following heating powers are
regarded as standards:--For olive oil, 55·5°; for cotton-seed, 69·5°
for nut, 62°; for sesamé, 66°; for poppy oil, 73°.
The application of Hubl’s test for butter (see p. 75) is one of the
most useful means for the detection of foreign oils in olive oil. The
iodine absorption number of the pure oil is considerably below that of
its most common adulterants.
The prevalence of the adulteration of olive oil has been abundantly
demonstrated. Of 232 samples examined by the New York and Massachusetts
State Boards of Health, 165 (71 per cent.) were spurious. It is a
notorious fact that large quantities of cotton-seed oil are exported
from the United States to France and Italy, much of which returns home
under the guise of the genuine product of the olive.
FOOTNOTES:
[136] It has been stated that American olive oil of superior excellence
is made in the States of N.C., Miss, and Cal.; but this product does
not, as yet, appear to be generally known on the New York market.
[137] Frens. Zeitsch. 3, 1864, p. 513.
MUSTARD.
Mustard is the product obtained by crushing and sifting the seeds of
_Sinapis nigra_ and _Sinapis alba_, of the genus Brassicaceæ. In the
manufacture of the condiment, both the black and white seeds are used.
According to analyses made by Piesse and Stansell,[138] fine grades of
the two varieties of mustard possess the following composition:--
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