How to become a scientist : $b Giving interesting and instructive experiments in chemistry, mechanics, acoustics and pyrotechnicsWarford, Aaron A.
Science
How to become a scientist : $b Giving interesting and instructive experiments in chemistry, mechanics, acoustics and pyrotechnics
Warford, Aaron A.
Scientific recreations
Gases are for the most part transparent and colorless, with a few
exceptions, and of course, like the air of the atmosphere, invisible.
They are little affected by the attraction of cohesion, but rather, on
the contrary, the particles composing them have a constant tendency
to separate from each other, so that their force of expansion is
only limited by the pressure under which they may be kept, and the
temperature they may be exposed to. They have a tendency to _penetrate_
each other, as it were; for instance, if you take a jar of heavy gas,
such as carbonic gas, set it with its mouth upwards, then invert over
it another jar containing hydrogen, a gas nearly twenty-two times
lighter, in a very short time the two gases will have become thoroughly
mixed, the heavy carbonic acid having risen, and the light hydrogen
fallen, until the gases are thoroughly mixed, each jar containing an
equal quantity of each gas.
Oxygen Gas.
This gas, so named from two Greek words signifying the maker of acid,
was discovered by Dr. Priestly in 1774. He obtained it by heating
the red oxide of mercury in a glass retort, when the gas escaped in
considerable quantities. In the ensuing year Scheele obtained it by a
variety of methods, and a few years afterwards Lavoisier discovered
that it was contained in atmospheric air, where it exists in the
proportion of about one-fifth, the remaining four fifths being almost
entirely nitrogen.
Oxygen gas may be obtained for the purpose of experiment, by heating to
redness the black oxide of manganese in an iron bottle, to the mouth of
which a flexible tube is attached to convey away the gas as fast as it
is liberated from the manganese. The first portions should be allowed
to escape, being mixed with the air in the tubes and bottle, and the
remainder may be collected in a gasometer, or in glass jars inverted
over water.
Another method to obtain the gas, and one to be used only in the
absence of other ingredients, is to mix in a retort some of this same
oxide of manganese with about half its weight of strong sulphuric
acid, and apply heat to the retort, when the gas will come over in
considerable quantities; the first portions must be allowed to escape
as before.[1] If the gas is required very pure, a small quantity of the
salt called chlorate of potassa, may be heated in a retort, and oxygen
gas will be evolved, and may be collected as before. If you have an
iron bottle, the first mode is by far the cheapest, as the heat of a
bright fire is sufficient for the operation, and a large quantity of
gas is obtained in a short time from a very inexpensive material. The
most rapid and convenient process of all is to heat a mixture of two
parts chlorate of potash, and one of powdered black oxide of manganese,
in a common clean oil flask, to which a cork and bent tube has been
adapted. Care must be taken not to mistake sulphide of antimony for
black oxide of manganese, as very serious accidents have arisen from
this cause.
Public-domain text, read in full here on John Shaqi.
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