Legal Chemistry: A Guide to the Detection of Poisons, Examination of Tea, Stains, Etc., as Applied to Chemical JurisprudenceNaquet, Alfred
Science
Legal Chemistry: A Guide to the Detection of Poisons, Examination of Tea, Stains, Etc., as Applied to Chemical Jurisprudence
Naquet, Alfred
Chemistry, Forensic; Poisons
in the sample can be estimated by the relative distance which the plates
have been separated.
[T] The British Society of Public Analysts regard the following as the
_minimum_ proportions of constituents in unadulterated milk:
Fat 2.5 per cent.
Solids, not fat 9. " "
----
Total 11.5 " "
Water 88.5 " "
--_Trans._
The lactoscope possesses, however, but a limited degree of precision.
_M. Marchand_ substitutes to its use the following tests: A test-tube is
graduated in three equal divisions, the upper one being subdivided into
hundredths extending above, in order to determine accurately the correct
volume of the fluid, expanded, as it is, by the temperature of 40°, at
which the examination is executed. The first division of the tube is
filled with milk, a drop, or two of strong potassa lye added, and the
mixture well shaken: the second portion is then filled with ether, and
the third with alcohol. The mixture is next again thoroughly agitated,
and then exposed to a temperature of 40° in a water-bath. After standing
for several hours, a layer of fatty matter becomes sufficiently
separated to allow of measurement: but, as it contains some ether and as
a small amount of butter may still be retained in the lower aqueous
fluid, a correction of the results obtained is necessary. M. Marchand
has compiled a table, which facilitates this correction (_vide_: _Journ.
de Pharm., Novembre 1854_, and _Bulletin de l'Académie de Médecine,
Paris, 1854_, xix., p. 1101).
Previously to the introduction of Marchand's apparatus, use was made of
the _lactometer_, which consists simply of a graduated glass tube, in
which the suspected milk is allowed to remain for 24 hours, at a
temperature of 15°. After the lapse of this time, the cream present
completely separates as a supernatant layer, the thickness of which
indicates the quality of the sample taken.
_M. Lacomte_ recommends the addition of glacial acetic acid, in order to
cause the more rapid separation of the cream.
Public-domain text, read in full here on John Shaqi.
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