Nitro-Explosives: A Practical TreatiseSanford, P. Gerald (Percy Gerald)
Science
Nitro-Explosives: A Practical Treatise
Sanford, P. Gerald (Percy Gerald)
Celluloid; Explosives
The heat test is performed as before, except that the temperature of the
bath is kept at 170 deg. F. (66 deg. C.), and regulator set to maintain that
temperature. Twenty grains (1.296 grm.) are used, placed in the test tube,
gently pressed down until it occupies a space of as nearly as possible
1-5/10 inch in the test tube of dimensions previously specified. The fine
cotton adhering to the sides of the tube can be removed by a clean cloth
or silk handkerchief. The paper is moistened by touching the upper edge
with a drop of the 50 per cent. glycerine solution, the tube inserted in
the bath to a depth of 2-1/2 inches, measured from the cover, the
regulator and thermometer being inserted to the same depth. The test paper
is to be kept near the top of the test tube, but clear of the cork, until
the tube has been immersed for about five minutes. A ring of moisture will
about this time be deposited upon the sides of the test tube, a little
above the cover of the bath. The glass rod must then be lowered until the
lower margin of the moistened part of the paper is on a level with the
bottom of the ring of moisture in the tube. The paper is now closely
watched, The test is complete when a very faint brown coloration makes its
appearance at the line of boundary between the dry and moist parts of the
paper. It must stand the test for not less than ten minutes at 170 deg. F.
(The time is reckoned from the first insertion of the tube in the bath
until the appearance of a discoloration of the test paper.)
~B. Schultze Powder, E.C. Powder, Collodion-Cotton, &c.~--The sample is
dried in the oven as above for fifteen minutes, and exposed for two hours
to the air. The test as above for compressed gun-cotton is then applied.
~C. Cordite~ must stand a temperature of 180 deg. F. for fifteen minutes. The
sample is prepared as follows:--Pieces half an inch long are cut from one
end of every stick selected for the test: in the case of the thicker
cordites, each piece so cut is further subdivided into about four
portions. These cut pieces are then passed once through the mill, the
first portion of material which passes through being rejected on account
of the possible presence of foreign matter from the mill. The ground
material is put on the top sieve of the nest of sieves, and sifted. That
portion which has passed through the top sieve and been stopped by the
second is taken for the test. If the mill is properly set, the greater
portion of the ground material will be of the proper size. If the volatile
matter in the explosive exceeds 0.5 per cent., the sifted material should
be dried at a temperature not exceeding 140 deg. F, until the proportion does
not exceed 0.5 per cent. After each sample has been ground, the mill must
be taken to pieces and carefully cleaned. The sieves used consist of a
nest of two sieves with holes drilled in sheet copper. The holes in the
top sieve have a diameter = 14 B.W.G., those in the second = 21 B.W.G.
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