Nitro-Explosives: A Practical TreatiseSanford, P. Gerald (Percy Gerald)
Science
Nitro-Explosives: A Practical Treatise
Sanford, P. Gerald (Percy Gerald)
Celluloid; Explosives
Some method of measuring the quantity of glycerine used must be adopted. A
gauge-tube graduated in inches is a very good plan, but it is essential
that the graduations should be clearly visible to the operator upon the
platform in front of the apparatus. A large tap made of earthenware (and
covered with lead) is fixed in the side of the nitrating tank just above
the bottom, to run off the charge after nitration. This should be so
arranged that the charge may be at option run down the conduit to the next
house or discharged into a drowning tank, which may sometimes be necessary
in cases of decomposition. The drowning tank is generally some 3 or 4
yards long and several feet deep, lined with cement, and placed close
outside the building.
The apparatus having received a charge of mixed acids, the water is
started running through the pipes coiled inside the tank, and a slight
pressure of compressed air is turned on,[A] to mix the acids up well
before starting. The nitration should not be commenced until the two
thermometers register a temperature of 18 deg. C. The glycerine tap is then
partially opened, and the glycerine slowly admitted, and the compressed
air turned on full, until the contents of the apparatus are in a state of
very brisk agitation. A pressure of about 40 lbs. is about the minimum (if
247 lbs. of glycerine and 16 cwt. of acids are in the tank). If the
glycerine tube is fitted with an injector, it may be turned on almost at
once. The nitration will take about thirty minutes to complete, but the
compressed air and water should be kept on for an additional ten minutes
after this, to give time for all the glycerine to nitrate. The temperature
should be kept as low as possible (not above 18 deg. C.).
[Footnote A: At the Halton Factory, Germany, cylinders of compressed
carbon dioxide are connected with the air pipes so that in the event of a
failure of the air supply the stirring can be continued with this gas if
necessary.]
The chief points to attend to during the progress of the nitration are--
1. The temperature registered by the two thermometers.
2. The colour of the nitrous fumes given off (as seen through the little
window in the dome of the apparatus).
3. The pressure of the compressed air as seen from a gauge fixed upon the
air pipe just before it enters the apparatus.
4. The gauge showing the quantity of glycerine used. The temperature, as
shown by either of the two thermometers, should not be at any time higher
than 25 deg. C.
If it rises much above this point, the glycerine should be at once shut
off, and the pressure of air increased for some few minutes until the
temperature falls, and no more red fumes are given off.
The nitration being finished, the large earthenware tap at the bottom of
the tank is opened, and the charge allowed to flow away down the conduit
to the next building, i.e., to the separator.
Public-domain text, read in full here on John Shaqi.
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