Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
Certain aromatic substances that occur in large amounts in some
parts of plants, are best obtained by pressure. The rinds of certain
fruits contain an essential oil in considerable quantities inclosed
in receptacles easily distinguished under the microscope. When these
vegetable substances are subjected to strong pressure, the oil
receptacles burst and the essential oil escapes. The force is usually
applied through a screw press with a stout iron spindle; the vegetable
substances being inclosed in strong linen or horse-hair cloths, placed
between iron plates, and subjected to a gradually increasing pressure.
Comparative experiments have shown us that even with the most powerful
presses a considerable, amount of oil is lost owing to the fact that a
large number of oil receptacles remain intact. For this reason, when
oil is to be extracted by pressure, a hydraulic press is preferable,
as it develops greater power than any other press. In the hydraulic
presses used for this purpose the piston fits exactly into a hollow
iron cylinder with sieve-like openings in its circumference. The
vegetable substances are filled into this cylinder; when the pressure
is applied, the fluids escape through the perforations, and the
residue forms a compact woody cake which is then free from oil.
Besides the essential oil, watery fluid is expressed, the whole
appearing as a milky liquid, owing to the admixture of vegetable
fibres, mucilage, etc. It is collected in a tall glass cylinder which
is set in a place free from any vibration. After remaining at rest for
several hours the liquid separates into two layers, the lower being
watery and mixed with mucilage, that floating on top being almost
pure oil. The latter is separated, and finally purified by filtration
through a double paper cone in a funnel covered with a glass plate.
[Illustration: FIG. 4.]
It is best to separate the water and oil in a regular separatory
funnel, or in a simple apparatus illustrated in Fig. 4. It is made
by cutting the bottom from a tall flask, and fitting into the neck
by means of a cork a glass tube having a diameter of one-fourth to
one-half inch. A rubber tube with stop-cock is fastened to the glass
tube. By careful opening of the stop-cock, the watery fluid can be
drained off to the last drop.
To the perfumer this method is of little importance, since it is
applicable only to a few substances which, moreover, give cheap odors.
Still, the possession of a hydraulic press is advisable to every
manufacturer who works on a large scale, as it is useful also in the
preparation of several fixed oils frequently employed in perfumery, for
instance, oils of almonds, nuts, etc.
[Illustration: FIG. 5.]
[Illustration: FIG. 6.]
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