Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
The water in K is heated until the contents of B are in brisk
ebullition; the vapor rises through RH, is condensed on entering E and
falls in small drops on the material. This fine rain of the solvent
dissolves the aromatic substances and flows back into B, where it is
again evaporated, and so on.
At the end of the extraction the faucets H and H_{1} are closed and
H_{2}, is opened. The vapors of the solvent pass through it into a worm
where they are condensed; the essential oil remaining in B is drained
off by opening H_{3}.
For still larger operations more perfect apparatuses are employed,
such as those of Seiffert and Vohl. Seiffert’s apparatus (Fig. 24)
consists of a battery of jacketed cylinders; steam circulates in the
space between the cylinders and the jackets. Each cylinder contains a
plate covered with a wire net on which the flowers to be extracted are
placed. All the cylinders having been filled and closed, the solvent is
admitted from a container above, through S and _a_ into C^2; when this
is filled the liquid flows through _a_^2_b_^3_c_^n into C. The solution
saturated with essential oil leaves the apparatus through _d_^n and
_p_ and enters a reservoir. The course of the liquid is aided by the
suction of an air-pump acting on _p_.
When the reservoir contains an amount of fluid equal to that in C^n,
_d_^n is closed, _a_^n is opened, and C connected with C^1 through
_b_^n and _c_^1. That the contents of C^2 are completely extracted is
shown by the fact that the liquid appears colorless in the glass tube
inserted in _b_^2; _a_^1 and C^2 are closed; _a_^2 and C^3 are opened,
thereby excluding C^2 from the current of bisulphide of carbon which
then flows through C^3C^nC^1. In order to permit the free flow of
the bisulphide of carbon through S despite the exclusion of C^2, the
faucets _a_^1_a_^2_a_^3_a_^n must be two-way cocks; in one position
they connect S with _b_; in the other they close _b_ and leave the
passage through S open.
[Illustration: FIG. 24.]
In order to collect the bisulphide of carbon present in the extracted
residue in C^2, faucet _g_^2 is opened and the bisulphide of carbon
allowed to escape through _h_. The faucet _e_^2 in tube L on being
opened admits compressed air to C^2, thus hastening the outflow. If
nothing escapes below, faucets _f_^2 and _f_^x are opened, steam enters
through tube D between jacket and cylinder; the bisulphide of carbon
vapor passes through _g_^2 and _h_ into the worm. After the expulsion
of the bisulphide of carbon, C^3 is emptied, refilled, connected with
C^1, and bisulphide of carbon admitted from C^3 in the manner above
described.
An extraction apparatus which has been much recommended of late is the
so-called “Excelsior Apparatus” made by Wegelin and Huebner, Halle a.
S., which can be worked with any desired solvent. The construction of
the apparatus (Figs. 25 and 26) is as follows.
[Illustration: FIG. 25.]
[Illustration: FIG. 26.]
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