Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
The solvent is admitted to the reservoir R in the lower part of the
condenser B through the tube indicated in the figure. The material
to be extracted having been filled into the cylinder A through the
manhole, the apparatus is closed. The cold water is admitted to the
condenser by opening a faucet. The three-way cock shown in Fig. 25 is
so placed as to open a communication of the overflow tube with A. The
faucet at the lower end of the reservoir R is now opened sufficiently
and the solvent passes into A from above, and as it descends takes
up more and more oil, flows through the sieve-plate, and escapes
through the tube at the bottom of A through the three-way cock, the
overflow tube, and the drain tube into the accumulator C. The opening
of a faucet now admits steam to the heating coil, when the solvent
evaporates, leaving the oil or fat behind. It is condensed in B,
again returns to R, whence it passes once more through the faucet
into the extractor A. The vessel C and the tubes leading to A and C
are surrounded with felt to prevent loss of heat. A sample taken from
the small cock at the foot of A (it has a small plate in the interior
of the tube) will show when the extraction in A may be looked upon as
finished. The solvent is distilled off or recovered from the residue
in A in the following manner. First the faucet in R is closed. The
three-way cock A is set to establish direct communication between A and
C, thus cutting off the overflow tube. Hence all the solvent in A flows
into C for distillation, while the oil is left behind. Steam being
admitted to the residue, the solvent rises as vapor through the upper
tube from A to B and collects in a liquid state in R. To drive off the
last traces of the solvent from the fat or oil obtained, steam is blown
into C by opening the valve. Besides the solvent, watery vapor enters B
and forms a layer of water in R under the solvent. By taking a sample
from the test-cock of the reservoir C which has an internal small
plate, the termination of the process is ascertained. The gauge tube at
the reservoir shows the level of the solvent and water. The water is
drawn off by opening the faucet at the lower end of the reservoir. A is
emptied through the manhole and by draining the oil from C through the
discharge cock. The tube R is closed by a light valve so as to prevent
evaporation of the solvent. All the apparatuses work without pressure
so that there is no danger from overstrain.
[Illustration: FIG. 27.]
[Illustration: FIG. 28.]
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