Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
After the solvent has been distilled off, the less volatile essential
oil remains in the still almost pure, containing only traces of wax,
vegetable fat or coloring matter which are of no consequence for our
purposes. The last remnants of the solvent cannot be expelled by
distillation, but by forcing through the essential oil a current of
pure air for fifteen or twenty minutes. The essential oils then are of
the purest, unexceptionable quality.
[Illustration: FIG. 30.]
In the case of delicate oils it is better to use carbonic acid in place
of air for expelling the last traces of the solvent, as the oxygen
may impair the delicacy of the fragrance. For this purpose we use the
apparatus illustrated in Fig. 30. In the large bottle A carbonic acid
is generated by pouring hydrochloric acid over fragments of white
marble. The carbonic acid passes into the vessel B filled with water
which frees it from any adhering drops of hydrochloric acid; then into
C filled with sulphuric acid to which it yields its water so that only
pure carbonic acid escapes through the fine rose at the end of tube
D which is made of pure tin, and as it passes through the oil in E
it carries off the last traces of the volatile solvent. In its final
passage through the water in F it leaves behind any oil that may have
been carried with it.
As all the aromatic substances change in air by the gradual absorption
of oxygen, and lose their odor—become resinified—these costly
substances must be put into small bottles which they completely
fill, and be preserved in a cool dark place, as light and heat favor
resinification. The bottles must be closed with well-fitting glass
stoppers.
Aromatic waters or eaux aromatisées, such as jasmine water (eau de
jasmin), orange-flower water (eau de fleurs d’oranges, eau triple de
Néroli, aqua naphæ triplex), etc., are made by distillation of these
flowers with water and show a faint but very fine odor. When they
contain, besides, dilute alcohol they are called spirituous waters
or esprits. Those brought into commerce from southern France are of
excellent quality.
THE YIELD OF ESSENTIAL OILS.
The quantities of essential oil obtainable from the vegetable
substances vary with the amount present in each. The following table
shows the average quantities of oil to be obtained from 100 parts of
material.
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