Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
The solutions of the essential oils in bisulphide of carbon are
distilled off in the steam still illustrated in Fig. 27; the steam
enters at _h_, the water of condensation escapes at _d_, the liquid
to be distilled enters at _e_ from a container at a higher level. The
boiling is kept uniform by the stirring arrangement _hg_. After the
bisulphide of carbon is distilled off, air is passed through the oil by
the curved tube _a_ which has fine perforations, so as to evaporate the
last traces of the solvent.
In Vohl’s apparatus (Fig. 28), arranged for petroleum ether, the
extraction is effected with the boiling fluid; hence this apparatus
is better adapted for the cheaper oils than for the finest oils from
flowers. The apparatus consists of two extractors A A, the accumulator
B, and the condenser C. Petroleum ether is allowed to flow over the
substances to be extracted, by opening the faucets _mm_, _vh_, closing
_ogw_E, and opening _o_, the course being through _ux_ to B. When B
is two-thirds full, the flow of petroleum ether is cut off, steam
is admitted through _y_ and the contents of B are brought to the
boiling-point. The vapors pass through _g_ and are condensed in _f_
until the contents of A reach the boiling-point of the solvent, when
the vapors pass through _i_ into C, and after closing _m´_ the liquid
passes through _ml_ into the inner cylinder of the extraction apparatus
and returns through _uxx_.
After the contents of A are extracted, _m´_ is opened, _m_ closed, and
steam is admitted through _d_ into the jacket of A; the vapors of the
solvent force the liquid part of the contents through _ux_ into B.
Overfilling of B is prevented by allowing the vapors of the solvent to
escape at the proper time into the condenser through _p_ by opening
_q_. Then _v_ is closed, _q_ opened, and the steam present in A drawn
off by an exhaust applied to _p_; as soon as _p_ begins to cool, all
the petroleum ether is distilled off, the steam is cut off at _d_, and
the extract evacuated through _t_. The contents of B are brought into a
still through D and E.
[Illustration: FIG. 29.]
By employing greater pressure the extraction can also be effected by
what is called displacement; the material to be extracted is placed
in a stout-walled vessel S (Fig. 29) which is connected by a narrow
tube at least ten yards long with the vessel F containing the solvent.
Stopcock H is first opened, then stop-cock H_{1} which is closed as
soon as fluid begins to flow from it. After the liquid has remained in
contact with the material for from thirty to sixty minutes, H_{1} is
opened very slowly, the liquid is allowed to escape and is displaced
with water which is made to pass out of F in the same way as the
solvent, until the latter is completely displaced from S.
Public-domain text, read in full here on John Shaqi.
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