Philosophical transactions, Vol. L. Part I. For the year 1757.: Giving some account of the present undertakings, studies, and labours, of the ingenious, in many considerable parts of the world.Various
History
Philosophical transactions, Vol. L. Part I. For the year 1757.: Giving some account of the present undertakings, studies, and labours, of the ingenious, in many considerable parts of the world.
Various
Science -- Periodicals
I imagined, that when the water was boiled with milk, the mixture would
have become of a muddy yellow colour, by the separation of the ochre:
but it did not even appear, that the ochre was at all separated from
the mixture, as it is from the water when boiled by itself. On the
contrary, not only the coagulum, but also the liquor, was of a pure
white colour, and of a pleasant taste: and this makes me think it worth
the inquiring into, whether or not the water does retain its medical
qualities after it is prepared in this manner with milk? For, if it
does, such a preparation might certainly be very serviceable in many
cases.
These experiments, which we next relate, do not only ascertain the
existence of alum in the water with greater certainty, but also, that
there is a particular kind of earth conjoined with this salt.
_Exp._ 26. An English quart of the water being kept boiling for
a quarter of an hour, it turned thick, muddy, and yellow, by the
separation of its ochrous parts; and, being set to cool in a clean
bowl, the next day all the ochre was subsided to the bottom, from which
the water was carefully filtred: whereby it became almost as clear and
limpid as before the elixation, retaining a sharp aluminous taste, but
was deprived of the strong ferrugineous taste, which it had at first.
This water was again boiled; by which means it was again turned a
little yellow, by the separation of some more ochre. It was therefore
again filtred, and rendered clear, and its aluminous taste was stronger
than before. After this filtration, the water was evaporated in a
sand-heat to about a sixteenth part of the original quantity, and then
it tasted like a strong solution of alum joined with a small degree of
a chalybeat taste. And this being totally evaporated in a glass, there
adhered upon its sides a pure white salt; and a larger quantity of the
same salt remained in the bottom of the glass, which was not so white,
but more impure than the former, and of a brown colour.
27. This salt, thus procured from the water, being mixed with distilled
vinegar and spirit of vitriol, there was not the least effervescence
produced.
28. Some of the brown-coloured salt being put upon a red-hot iron, it
did neither sparkle nor decrepitate; but was turned into a blackish
cineritious substance, which in a short time became a white calx. And
tho’ some of the salt was put upon the iron finely powdered, yet it
concreted, and run together in a cinder, whose cohesion was afterwards
destroyed when calcined by a further degree of heat.
29. As I was accidentally deprived of the opportunity of obtaining
crystals of this salt, which would have been the best means of knowing
to what species it was to be referred; I dissolved the whole mass in
a small quantity of spring-water, and, by filtrating this solution, I
obtained a large proportion of fine earth of a brown colour.
30. This solution of the salt afforded a deep blue tincture with galls.
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