The solutions should be approximately tenth normal, the actual strength
in each case being determined by analysis. The phosphorus is determined
as magnesium pyrophosphate in the usual way, the potash as potassium
platinochlorid, the ammonia by collecting the distillate from soda in
half normal hydrochloric acid and titrating with standard alkali, and
the nitrate by Warington’s modification of Schlösing’s method for gas
analysis. The details of these methods of determination will be given
later. One hundred grams of the sifted, air-dried soil are placed in a
rubber stopped bottle and treated with 250 cubic centimeters of the
solution to be tested. The digestion is continued for forty-eight hours
in each case, the bottles being thoroughly shaken at the end of
twenty-four hours. At the end of the treatment the solutions are
filtered and the salts determined in aliquot portions. The details of
this method are essentially those already described.
=137. Statement of Results.=—Duplicate analyses should be made and the
tabulation of the data is illustrated in the following analyses by
Huston:
Na₂HPO₄ cubic Weight of Weight of P₂O₅ Salt
centimeters Mg₂P₂O₇ in Mg₂P₂O₇ in absorbed removed
filtrate taken. twenty-five filtrate. by 100 per
cubic grams cent.
centimeters of soil.
the solution.
(a) 25 0.1368 gram 0.0962 gram
(b) 25 0.0963 „ 0.2589 29.6
gram
——————
Mean 0.0963 „
KCl cubic Weight of Weight of K₂O Salt
centimeters K₂PtCl₆ in K₂PtCl₆. absorbed removed
filtrate taken. twenty-five by 100 per
cubic grams cent.
centimeters of soil.
solution.
(a) 25 0.6154 gram 0.4505 gram
(b) 25 0.4540 „ 0.3161 26.5
gram
——————
Mean 0.4523 „
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