The same process is applied to the separation of silt from dust. When
all the silt has been removed from the dust and clay, the turbid water
containing the dust and clay is set aside and allowed to settle in a
cylindrical vessel for twenty-four hours. The vessel is filled to a
height of 200 millimeters. According to Hilgard, the separation of the
dust from clay during a subsidence of twenty-four hours, will give
results of sufficient accuracy, although the clay then remaining
suspended will not be entirely free from measurable fine particles up to
0.001 or 0.002 millimeter diameter.
Small beakers and small quantities of distilled water are used at first
for the decantations, as thus the duration of subsidence is less and
more decantations can be made in a given time than when larger
quantities of water are employed. Beakers of about 100 cubic centimeters
capacity are convenient for the coarser grades, but it is necessary to
use larger vessels for the fine sediments from which turbid water
accumulates that cannot be thrown away, as may be done with the clear
water, from which the coarse sediments settle out completely in a short
time.
It is best to keep the amount of water as small as possible in working
out the dust since loss is incurred in using too large quantities.
It is also necessary in most cases to subject the various fractions
obtained during elutriation, to careful kneading with a soft rubber
pestle so that the fine lumps of clay may be broken up and caused to
remain suspended in the water. This treatment with the pestle should be
done in such a way as to avoid as far as possible all grinding of the
particles, the object being merely to pulverize the minute aggregations
of clay and extremely fine particles which always form on drying a
sample of soil after removing it from the ground.
_Measurement of the Particles._—To determine the size of particles in
suspension, a small glass tube is applied to the surface of the liquid
in such a way as to take up a single drop which is transferred to a
glass slide. This drop will contain the smallest particles in the
liquid.
To obtain a sample of the coarsest particles the liquid is allowed to
stand long enough to form a very slight sediment and a portion of this
sediment is collected with a glass tube.
To determine the diameter of the particles in a sediment it is stirred
vigorously with a little water and the pipette at once applied to the
surface of the water. On decanting the greater part of the sediment, the
large particles remain at the bottom of the beaker and may be easily
examined.
_Time._—The time required to make the separations, above described, is
about two hours for each, so that an analysis including the sittings, is
made in five or six hours, exclusive of the time necessary for
collecting the dust and separating the clay, for which a subsidence of
twenty-four hours is allowed.
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