_Weighing the Sediments._—The sediments are prepared for weighing by
allowing them to subside completely, decanting the clear water as far as
possible, rinsing them into a weighed platinum dish and igniting. The
dish is cooled in a desiccator.
_Effect of Boiling._—The analyses show a very decided increase in the
particles smaller than 0.01 millimeter diameter at the expense of
coarser particles as the result of boiling. The surfaces of the coarser
particles are seen to be polished and of a lighter color than those not
boiled. The surfaces of the unboiled particles are coated with a film of
fine material probably cemented to them by clay. When these coarse
particles which have not been boiled, are violently stirred with water
for a short time, no fine particles are detached from them; and a
careful examination under the microscope fails to reveal in any of the
sediments more than an occasional grain exceeding the 0.05 millimeter
limit by so much as 0.01 millimeter, or the 0.01 limit by as much as
0.005 millimeter. It would, therefore, appear that these small particles
thus set free by long boiling are really a part of the larger ones and
should be treated as such in a mechanical analysis of these soils.
=209. The French Method.=—The Schloesing method[142] as practiced by the
French agricultural chemists[143] differs essentially from those already
described in attempting to first free the silt from carbonates and
organic matter. It is conducted as follows:
One kilogram of the soil previously dried in the air, is taken and
passed through a sieve of which the meshes are five millimeters. The
agglomerated particles of earth are broken up by the hand. The pebbles
are also taken out and weighed. The pebbles are then treated with
hydrochloric acid until all effervescence is over. The insoluble part is
dried and again weighed. The difference in weight gives the quantity of
calcium carbonate contained on the external surface of the pebbles. The
earth which passes the sieve of five millimeters mesh is next passed
through a sieve having ten meshes to the centimeter. The masses on the
sieve are broken up with the hand or with a pestle, in such a manner as
to separate the fine agglomerated particles. The material which remains
upon the sieve after being dried at 100°, is weighed. This gives the
coarse sand. This is treated with hydrochloric acid as were the pebbles
before, washed and the residue dried and weighed. The difference in
weight gives the quantity of calcium carbonate adhering to the surface
of the coarse sand.
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