=14. Drying In a Closed Water Oven.=—When it is desired to keep the
temperature of a drying oven exactly at 100° instead of at the heat of
boiling water, a closed water oven with a thermostat is to be employed.
The oven should be so constructed as to secure a free circulation of
the water about the inner space. Since as a rule the water between the
walls of the apparatus will be subjected to a slight pressure, these
walls should be made strong, or the cylindrical form of apparatus
should be used. The thermostat used by the Halle Station is shown in
Fig. 6.[4] A =⋃= shaped tube, with a bulb on one arm and a lateral
smaller tube sealed on the other, is partly filled with mercury and
connected by rubber tubes on the right with the gas supply, and on
the left with the burner. The end carrying the bulb is connected
directly by a rubber and metal tube with the water space of the oven.
This device is provided with a valve which is left open until the
temperature of the drying space reaches about 95°. The tube conducting
the gas is held in the long arm of the =⋃= by means of a cork through
which it passes air-tight and yet is loose enough to permit of its
being moved. Its lower end is provided with a long ▲ shaped slit.
When the valve leading to the water space is closed and the water
reaches the boiling point, the pressure of the vapor depresses the
mercury in the bulb arm of the =⋃= and raises it in the other. As the
mercury rises it closes the wider opening of the ▲ shaped slit, thus
diminishing the flow of gas to the burner. By moving the gas entry
tube up or down a position is easily found in which the temperature of
the drying space, as shown by the thermometer, is kept accurately and
constantly at 100°.
In a bath arranged in this way a steam condenser is not necessary.
Since, however, in laboratories which are not at a higher altitude than
1,000 feet the boiling-point of water is nearly 100°, it does not seem
necessary to go to so much trouble to secure the exact temperature
named. There could be no practical difference in the percentage of
moisture determined at 100°, and at the boiling-point of water at a
temperature not more than 1° lower.
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