=300. Variations in the Instruments.=—In the use of the
oleorefractometer, attention should be called to the fact that, through
some negligence in manufacture, the instruments do not give, in all
instances, the same reading with the same substance. Allen obtained the
following data with a sample of lard examined in three instruments,
_viz._, 4°.5, 6°, and 11°. Such wide differences in the scales of
the instruments cannot fail to disparage the value of comparative
determinations.
The variations in samples of known origin, when read on the same
instrument, however, will show the range of error to which the
determinations made with the oleorefractometer are subject. Pearmain
has tabulated a large number of observations of this kind, covering 240
samples of oils.[253]
Following are the data relating to the most important oils.
AT 22°.
Highest Lowest Mean
reading. reading. reading.
Name of oil. Degrees. Degrees. Degrees.
Almond 10.5 8.0 9.5
Peanut 7.0 5.0 6.0
Castor 42.0 39.0 40.0
Codliver 46.0 40.0 44.0
Cottonseed (crude) 17.0 16.0 16.5
” (refined) 23.0 17.0 21.5
Lard oil -1.0 0.0 0.0
Linseed (crude) 52.0 48.0 50.0
” (refined) 54.0 50.0 52.5
Olive 3.5 1.0 2.0
Rape 20.0 16.0 17.5
Sesamé 17.0 13.0 15.5
Sunflower 35.0 35.0 35.0
Tallow oil -5.0 -1.0 -3.0
Oleic acid -33.0 -29.0 -32.0
AT 45°.
Butter -34.0 -25.0 -30.0
Oleomargarin -18.0 -13.0 -15.0
Lard -14.0 -8.0 -10.5
Tallow -18.0 -15.0 -16.0
Paraffin 58.5 54.0 56.0
[Illustration: FIG. 94.—BUTYROREFRACTOMETER.]
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