=301. Butyrorefractometer.=—Another instrument graduated on an
arbitrary scale is the butyrorefractometer of Zeiss. This apparatus,
which resembles in some respects the instrument of Abbe, differs
therefrom essentially in dispensing with the revolving prisms of
Amici, whereby the chromatic fringing due to dispersion is corrected,
and on having the scale fixed for one substance, in this instance,
pure butter fat. The form of the instrument is shown in Fig. 94. The
achromatization for the butter fat is secured in the prisms between
which a film of the fat is placed, as in the Abbe instrument. When
a fat, differing from that for which the instrument is graduated is
introduced, the fringes of the dark and light portions of the field
will not only be colored (difference in dispersion), but the line of
separation will also be displaced (difference in refractive power). The
apparatus is therefore used in the differential determination of these
two properties. It must not be forgotten, however, that butter fats
differ so much in these properties among themselves as to make possible
the condemnation of a pure as an adulterated sample.
=302. Method of Charging the Apparatus.=—The prism casing of the
instrument is opened by turning the pin _F_ to the right and pushing
the half _B_ of the prism casing aside. The prism and its appendages
must be cleaned with the greatest care, the best means for this purpose
being soft clean linen moistened with a little alcohol or ether.
Melt the sample of butter in a spoon and pour it upon a small paper
filter held between the fingers and apply the first two or three drops
of clear butter fat so obtained to the surface of the prism contained
in prism casing _B_. For this purpose the apparatus should be raised
with the left hand so as to place the prism surface in a horizontal
position.
Press _B_ against _A_ and replace _F_ by turning it in the opposite
direction into its original position; thereby _B_ is prevented from
falling back and both prism surfaces are kept in close contact.
=303. Method of Observation.=—While looking into the telescope, give
the mirror _J_ such a position as to render the critical line which
separates the bright left part of the field from the dark right part
distinctly visible. It may also be necessary to move or turn the
instrument about a little. First it will be necessary to ascertain
whether the space between the prism surfaces be uniformly filled with
butter, for, if not, the critical line will not be distinct.
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