_Determination of Starch_, pp.
196-226.—Constitution of starch; Separation of
starch; Methods of separation; Separation with
diastase; Separation in an autoclave; Principles
of analysis; Estimation of water; Estimation of
ash; Estimation of nitrogen; Hydrolysis with acids;
Factors for calculation; Polarization of starch;
Solution at high pressure; Method of Hibbard;
Precipitation with barium hydroxid; Disturbing bodies
in starch determinations; Colorimetric estimation
of starch; Fixation of iodin; Identification of
starches; Vogel’s table; Muter’s table; Blyth’s
classification; Preparation of starches for the
microscope; Mounting in canada balsam; Description of
typical starches; Authorities cited in Part Second.
PART THIRD.
SEPARATION AND DETERMINATION OF CARBOHYDRATES IN
CRUDE OR MANUFACTURED AGRICULTURAL PRODUCTS.
_Sugars in Vegetable Juices_, pp.
227-253.—Introduction; Sugar in the sap of trees;
Sugar in sugar canes; Weighing pipettes; Gravimeter;
Reducing sugars in juices; Preservation of juices;
Direct estimation of sugar; Cutting or shredding
canes; Methods of analysis; Drying and extracting;
Examination of bagasse; Fiber in canes; Sugar beets;
Estimation of sugar in sugar beets; Machines for
pulping beets; Instantaneous diffusion; Pellet’s
process; Alcohol digestion; Extraction with alcohol;
Determination of sugar in mother beets; Determination
of sugars without weighing; Continuous observation tube.
_Analysis of Sirups and Massecuites_, pp.
254-264.—Specific gravity; Determination of water;
Determination of ash; Determination of reducing
sugars; Estimation of minute quantities of invert
sugar; Soldaini’s gravimetric method; Weighing the
copper as oxid; Analyses for factory control.
_Separation of Carbohydrates in Mixtures_, pp.
264-292.—Occurrence of sugars; Optical methods;
Optical neutrality of invert sugar; Separation of
sucrose and invert sugar; Separation of sucrose and
raffinose; Determination of levulose; Formula for
calculating levulose; Separation of sucrose from
dextrose; Estimation of lactose in milk; Error due
to volume of precipitate; Separation of sucrose,
levulose and dextrose; Sieben’s method; Wiechmann’s
method; Copper carbonate method; Winter’s process;
Separation with lead oxid; Analysis of commercial
glucose and grape sugar; Fermentation method;
Oxidation method; Removal of dextrose by copper
acetate; Separation of dextrin with alcohol.
_Carbohydrates in Milk_, pp. 293-298.—Copper
tartrate method; The official method; The copper
cyanid process; Separation of sugars in evaporated
milks; Method of Bigelow and McElroy.
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