=69. The Laurent Instrument.=—A polariscope adapted by Laurent to
the use of monochromatic yellow light is almost exclusively used in
France and to a considerable extent in this country. In case a worker
is confined to the use of a single instrument, the one just mentioned
is to be recommended as the best suited to general work. It has the
second nicol, called the analyzer, movable and the degree of rotation
produced is secured in angular terms directly on a divided circle. The
scale is graduated both in angular measurements and in per cents of
sugar for a definite degree of concentration of the solution and length
of observation tube. The normal solution in the laurent instrument
contains 16.19 grams of pure sugar in 100 true cubic centimeters, and
the length of the observation tube is 200 millimeters. Both the angular
rotation and the direct percentage of sugar can be read at the same
time. Great accuracy can be secured by making the readings in each
of the four quadrants. The light is rendered yellow monochromatic by
bringing into the flames of a double bunsen, spoons made of platinum
wire, which carry fragments of fused sodium chlorid.
[Illustration: FIGURE 33. LAURENT LAMP.]
=70. The Laurent Burner.=—The theory of the illumination of the laurent
burner is illustrated by the accompanying Fig. 33. The lamp consists
essentially of two bunsens, surmounted by a chimney.[38] A curved
spoon made of platinum gauze serves to hold the fused particles of
sodium chlorid which are used to produce the yellow light. The spoon
is shown at G, held by the arm F, fastened by the key P. The interior
intense flame B B is surrounded by an exterior less highly colored
flame A A. It is important that the optical axis of the polariscope
be directed accurately upon the disk B, which is the most intense
part of the illumination. The point of the spoon carrying the salt
should be coincident with the prolongation of the lamp TT, so that it
just strikes the edge of the blue flame. Care should be taken not to
press the spoons into the interior of the flame as by so doing the
intensity of the illumination is very much diminished. Great care must
be observed in the position of the spoon G, and the platinum arm F
being flexible, the operator with a little patience, will be enabled
to properly place the spoon by bending it. Moreover, if the spoon be
pressed too far into the flame, the melted particles of salt collecting
in the bottom of G may drop into the lamp and occlude the orifices
through which the gas enters. The light of the yellow flame produced by
the lamp may be further purified by passing through a prism filled with
a solution of potassium dichromate, or better, a homogeneous disk cut
from a crystal of that salt.
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