Scientific American Supplement, No. 360, November 25, 1882Various
Science
Scientific American Supplement, No. 360, November 25, 1882
Various
Science -- Periodicals
To fill the burette with gas, the three-way cock, _a_, is so placed that
the axial aperture shall be in communication with the graduated part, A,
of the burette. After this, water is poured into the funnel, t, and the
burette is put in communication with the gas reservoir by means of a
rubber tube. The lower point of the burette is put in communication with
a rubber pump, V (Fig. 2), on an aspirator (the cock, _b_, being left
open), and the gas is sucked in until all the air that was in the
apparatus has been expelled from it. The cocks, _a_ and _b_, are turned
90 degrees. The water in the funnel prevents the gases communicating
with the top. The point of the three-way cock is afterward closed with a
rubber tube and glass rod.
If the gas happens to be in the reservoir of an aspirator, it is made
to pass into the apparatus in the following manner: The burette is
completely filled with water, and the point of the three-way cock is
put in communication with a reservoir. If the gas is under pressure, a
portion of it is allowed to escape through the capillary tube into the
water in the funnel, by turning the cock, _a_, properly, and thus all
the water in the conduit is entirely expelled. Afterward _a_ is turned
180°, and the lower cock, _b_, is opened. While the water is flowing
through _b_, the burette becomes filled with gas.
_Mode of Measuring the Gases and Absorption_.--The tube that
communicates with the vessel, F, is put in communication, after the
latter has been completely filled with water, with the point of the
cock, _b_ (Fig. 2). Then the latter is opened, as is also the pinch cock
on the rubber tubing, and water is allowed to enter the burette through
the bottom until the level is at the zero of the graduation. There are
then 100 cubic centimeters in the burette. The superfluous gas has
escaped through the cock, _a_, and passed through the water in the
funnel. The cock, _a_, is afterward closed by turning it 90°. To
cause the absorbing liquid to pass into the burette, the water in the
graduated cylinder is made to flow by connecting the rubber tube, s, of
the bottle, S, with the point of the burette. The cock is opened, and
suction is effected with the mouth of the tube, r. When the water has
flowed out to nearly the last drop, _b_ is closed and the suction bottle
is removed. The absorbing liquid (caustic potassa or pyrogallate of
potassa) is poured into a porcelain capsule, P, and the point of the
burette is dipped into the liquid. If the cock, _b_, be opened, the
absorbing liquid will be sucked into the burette. In order to hasten
the absorption, the cock, _b_, is closed, and the burette is shaken
horizontally, the aperture of the funnel being closed by the hand during
the operation.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account