Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
These methods are intended to aid in determining the commercial
valuation of fats and fatty oils in their purchase and sale, based on
the fundamental assumption commonly recognized in the trade, namely,
that the product is true to name and is not adulterated. For methods for
determining the identity of oils and fats, the absence of adulterants
therein and for specific tests used in particular industries, the
chemist is referred to standard works on the analysis of fats and oils.
APPLICABILITY.
The methods are applicable in commercial transactions involving fats and
fatty oils used in the soap, candle and tanning industries, to edible
fats and oils and to fats and fatty oils intended for lubricating and
burning purposes. The methods are applicable to the raw oils used in the
varnish and paint industry with the exceptions noted under limitations,
but special methods have not been included.
LIMITATIONS.
The methods have not been developed with special reference to waxes
(beeswax, carnauba wax, wool wax, etc.) although some of them may be
found applicable to these substances. The Committee considers the Wijs
method superior to the Hanus method for the determination of iodine
number of linseed oil as well as other oils, although the Hanus method
has been considered standard for this work for some time and has been
adopted by the American Society for Testing Materials and in various
specifications. It has been customary to use the Huebl method for the
determination of iodine value of tung oil (China wood oil) but the
Committee's work indicates that the Wijs method is satisfactory for this
determination.
Sampling.
TANK CARS.
1. SAMPLING WHILE LOADING--Sample shall be taken at discharge of pipe
where it enters tank car dome. The total sample taken shall be not less
than 50 lbs. and shall be a composite of small samples of about 1 pound
each, taken at regular intervals during the entire period of loading.
The sample thus obtained is thoroughly mixed and uniform 3-lb. portions
placed in air-tight 3-lb. metal containers. At least three such samples
shall be put up, one for the buyer, one for the seller, and the third to
be sent to a referee chemist in case of dispute. All samples are to be
promptly and correctly labeled and sealed.
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