Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
(_b_) _When contents are liquid._ In this case use is made of a glass
tube with constricted lower end. This is inserted slowly and allowed to
fill with the liquid, when the upper end is closed and the tube
withdrawn, the contents being allowed to drain into the sample
container. After the entire sample is taken it is thoroughly mixed and
handled according to TANK CARS (1).
(_c_) _When contents are semi-solid._ In this case the tryer or a glass
tube with larger outlet is used, depending on the degree of fluidity.
(_d_) _Very hard materials, such as natural and artificial stearines._
By preference the barrels are stripped and samples obtained by breaking
up contents of at least 10 per cent of the packages. This procedure is
to be followed also in the case of cakes shipped in sacks. When shipped
in the form of small pieces in sacks they can be sampled by grab
sampling and quartering. In all cases the final procedure is as outlined
under TANK CARS (1).
2. DRUMS--Samples are to be taken as under (1), use being made of the
bunghole. The tryer or tube should be sufficiently long to reach to the
ends of the drum.
3. OTHER PACKAGES--Tubs, pails and other small packages not mentioned
above are to be sampled by tryer or tube (depending on fluidity) as
outlined above, the tryer or tube being inserted diagonally whenever
possible.
4. MIXED LOTS AND PACKAGES--When lots of tallow or other fats are
received in packages of various shapes and sizes, and especially wherein
the fat itself is of variable composition, such must be left to the
judgment of the sampler. If variable, the contents of each package
should be mixed as thoroughly as possible and the amount of the
individual samples taken made proportional to the sizes of the packages.
Analysis.
SAMPLE.
The sample must be representative and at least three pounds in weight
and taken in accordance with the STANDARD METHODS FOR THE SAMPLING OF
COMMERCIAL FATS AND OILS. It must be kept in an air-tight container, in
a dark, cool place.
Soften the sample if necessary by means of a gentle heat, taking care
not to melt it. When sufficiently softened, mix the sample thoroughly by
means of a mechanical egg beater or other equally effective mechanical
mixer.
MOISTURE AND VOLATILE MATTER.
APPARATUS: _Vacuum Oven_--The Committee Standard Oven.
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