True ground cinnamon (see Figs. 22 and 23, Chap. III) consists of long
cells of woody fiber which represent the thin layers found in the bark
and scattered through it, consisting of a little starch in stellate
cells. There is nothing more distinct between cinnamon and cassia than
the amount of volatile oil the bark contains, and yet some of the
inferior cinnamon bark does not contain as much volatile oil as does
good cassia, but cinnamon oil is of a much higher and more delicate
aroma. It is hard to detect cassia (see Fig. 41, Chap. III; adulterated,
Fig. 46) in ground cinnamon, as the flavor is so similar, but the cassia
contains but little wood fiber and few stellate cells and the presence
of starch is more marked. To test cinnamon, experts are required. The
usual test is by chewing, but this method soon makes the mouth sore. The
most inferior ground cassia, however, bears such a close resemblance to
the best cassia and to the true cinnamon that it may be substituted for
it or used as an adulterant without being easily detected. The following
instructions are useful in examining powdered cinnamon.
Make a decoction of pure ground cinnamon, also a decoction of the
suspected mixture, and filter both; when cold add to thirty grams of
each one or two drops of iodine, when the decoction of pure cinnamon
will be but slightly affected while the mixture will assume a
blackish-blue coloration. Although much depends upon the age of the
oils, the greater the age of the oil the smaller the quantity of iodine
solution absorbed by it. The cheap sort of cassia, or “Cassia Vera,” can
be distinguished from China cassia and from true cinnamon by its
richness in mucilage, which can be extracted by cold water as a thick
glary liquid, which on the addition of corrosive sublimate or neutral
acetate of lead yields a dense viscous precipitate. The most reliable
test for cassia in true cinnamon is to obtain the proportion of ash in
each, the ash in cinnamon being 4.59 and 4.78 per cent., cassia lignea
giving but 1.84 and “Cassia Vera” nearly the same as cinnamon, 4.08.
Another test is to ascertain the amount of ash soluble in water. The
quantities are 25.04, 28.98 per cent. in whole cinnamon, about 18 per
cent. in chips, and 8.15 in “Cassia Vera,” and 26.40 in cassia lignea.
Again the proportion of oxide of manganese is never more than 1 per
cent. (0.13-0.97) in cinnamon, but it is over (1.13-1.53) in “Cassia
Vera” and 3.65-5.11 in cassia lignea. The cinnamon ash will always be
found white or nearly so, while both the cassia ashes are gray or brown
and yield an abundance of chlorine on heating with hydrochloric acid.
The cinnamon or cassia in the bark is easily distinguished, as the
inferior kinds are thicker and appearance coarser and their color darker
brown and duller and have a more pungent taste, which is less sweet than
the true cinnamon, succeeded by a bitter taste.
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