Scorification consists in placing the ore in an open dish with proper reagents, and collecting all the volatile ingredients in the slag. Cupellation, on the other hand, collects them in the bone ash, of which the cupel is composed. When silver must be separated from gold, it is sometimes convenient to increase its proportion by the addition of some known weight of the inferior metal. After fusing, the globule is placed in nitric acid, and the silver parted from the gold, which may then be weighed. This result subtracted from the weight of the original globule gives the amount of silver. To test an ore for gold, take a pound of it, crush in mortar and pass through a fine sieve. Take one-fourth ounce Troy of the powder. Place in scorifier with an equal amount of litharge. Cover with borax that has been melted and powdered, and put the scorifier in the muffle of the furnace. A blacksmith's forge might do at a pinch. Heat until the mass has become a fluid, possibly twenty or thirty minutes. Next pour into the scorification mould, and, after the slag has set, remove it with a hammer. Hammer the button into a cube and place it in the cupel, which must first have been thoroughly heated. Heat until all the base metal has been absorbed by the cupel and the button has "brightened," or flashed; when this occurs, remove the cupel to the front of the muffle, cool, and remove the button with pincers. Weigh it, and you have the amount of gold and silver in 1/4-ounce Troy. A simple sum in proportion gives the amount in a ton. All ores containing sulphur, arsenic, antimony, or zinc, should be roasted. There are three stages in the scorification process; roasting, fusion, and scorification. During the first, the heat should be moderate until fumes cease to be given off; during the second, the heat is raised and a play of colors is seen on the surface of the lead; in the closing stage, the heat is lowered for a time until the slag covers the lead, when it is again raised for a short time and the scorifier removed. Brittle buttons may be due to arsenic, antimony, zinc or litharge, and must be re-scorified before cupellation, with more lead. Take the cupel slowly from the fire to avoid "spitting," by which portions of the buttons are lost. Watch closely for the brightening. Silver is volatile at a high heat, but when the muffle is almost white, the metal well fused and clean, the fumes rising slowly, and the cupel a cherry red, all is going smoothly. If the fumes rise rapidly, the muffle is too hot. On the other hand, dense, falling fumes show the temperature is too low. Lead that is poor in silver stands the highest heat without vitiating the assay. When the material in the cupel "freezes," i.e., the absorption by the cupel stops, reject the assay and try again, giving more heat or more lead.