The Art of Perfumery, and Methods of Obtaining the Odors of Plants: With Instructions for the Manufacture of Perfumes for the Handkerchief, Scented Powders, Odorous Vinegars, Dentifrices, Pomatums, Cosmetics, Perfumed Soap, Etc., to which is Added an Appendix on Preparing Artificial Fruit-Essences, Etc.Piesse, G. W. Septimus (George William Septimus)
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The Art of Perfumery, and Methods of Obtaining the Odors of Plants: With Instructions for the Manufacture of Perfumes for the Handkerchief, Scented Powders, Odorous Vinegars, Dentifrices, Pomatums, Cosmetics, Perfumed Soap, Etc., to which is Added an Appendix on Preparing Artificial Fruit-Essences, Etc.
Piesse, G. W. Septimus (George William Septimus)
Cosmetics; Perfumes
Take of finely-powdered litharge five pounds, and olive oil nine pounds.
Boil them together over a gentle fire, constantly stirring, with the
addition occasionally of a small quantity of warm water, until the
compound has the consistence of plaster. Jahn boils this plaster for
half an hour with an equal weight of water, keeping it at the same time
constantly stirred. When cold, he pours off the supernatant fluid, and
repeats the boiling three times at least with a fresh portion of water.
The sweet fluids which result are mixed, and evaporated to six pounds,
and sulphuretted hydrogen conducted through them as long as sulphuret
of lead is precipitated. The liquid filtered from the sulphuret of lead
is to be reduced to a thin syrupy consistence by evaporation. To remove
the brown coloring matter, it must be treated with purified animal
charcoal. However, this agent does not prevent the glycerine becoming
slightly colored upon further evaporation. It possesses also still a
slight smell and taste of lead plaster, which may be removed by diluting
it with water, and by digestion with animal charcoal, and some fresh
burnt-wood charcoal. After filtration, this liquid must be evaporated
until it has acquired a specific gravity of 1.21, when it will be found
to be free from smell, and of a pale yellow color. For the preparation
of glycerine, distilled water is necessary, to prevent it being
contaminated with the impurities of common water. Jahn obtained, by this
method, from the above quantity of lead plaster, upwards of seven ounces
of glycerine.--_Archives der Pharmacie_.
* * * * *
TEST FOR ALCOHOL IN ESSENTIAL OILS.
J.J. Bernoulli recommends for this purpose acetate of potash. When to an
ethereal oil, contaminated with alcohol, dry acetate of potash is added,
this salt dissolves in the alcohol, and forms a solution from which the
volatile oil separates. If the oil be free from alcohol, this salt
remains dry therein.
Public-domain text, read in full here on John Shaqi.
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