The Art of Perfumery, and Methods of Obtaining the Odors of Plants: With Instructions for the Manufacture of Perfumes for the Handkerchief, Scented Powders, Odorous Vinegars, Dentifrices, Pomatums, Cosmetics, Perfumed Soap, Etc., to which is Added an Appendix on Preparing Artificial Fruit-Essences, Etc.Piesse, G. W. Septimus (George William Septimus)
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The Art of Perfumery, and Methods of Obtaining the Odors of Plants: With Instructions for the Manufacture of Perfumes for the Handkerchief, Scented Powders, Odorous Vinegars, Dentifrices, Pomatums, Cosmetics, Perfumed Soap, Etc., to which is Added an Appendix on Preparing Artificial Fruit-Essences, Etc.
Piesse, G. W. Septimus (George William Septimus)
Cosmetics; Perfumes
Wittstein, who speaks highly of this test, has suggested the following
method of applying it as the best:--In a dry test-tube, about half an
inch in diameter, and five or six inches long, put no more than eight
grains of powdered dry acetate of potash; then fill the tube two-thirds
full with the essential oil to be examined. The contents of the tube
must be well stirred with a glass rod, taking care not to allow the salt
to rise above the oil; afterwards set aside for a short time. If the
salt be found at the bottom of the tube dry, it is evident that the oil
contains no spirit. Oftentimes, instead of the dry salt, beneath the oil
is found a clear syrupy fluid, which is a solution of the salt in the
spirit, with which the oil was mixed. When the oil contains only a
little spirit, a small portion of the solid salt will be found under the
syrupy solution. Many essential oils frequently contain a trace of
water, which does not materially interfere with this test, because,
although the acetate of potash becomes moist thereby, it still retains
its pulverent form.
A still more certain result may be obtained by distillation in a
water-bath. All the essential oils which have a higher boiling-point
than spirit, remain in the retort, whilst the spirit passes into the
receiver with only a trace of the oil, where the alcohol may be
recognized by the smell and taste. Should, however, a doubt exist, add
to the distillate a little acetate of potash and strong sulphuric acid,
and heat the mixture in a test-tube to the boiling-point, when the
characteristic odor of acetic ether will be manifest, if any alcohol be
present.
* * * * *
DETECTION OF POPPY AND OTHER DRYING OILS IN ALMOND AND OLIVE OILS.
It is known that the olein of the drying oils may be distinguished from
the olein of those oils which remain greasy in the air by the first not
being convertible into elaidic acid, consequently it does not become
solid. Professor Wimmer has recently proposed a convenient method for
the formation of elaidin, which is applicable for the purpose of
detecting the adulteration of almond and olive oils with drying oils. He
produces nitrous acid by treating iron filings in a glass bottle with
nitric acid. The vapor of nitrous acid is conducted through a glass tube
into water, upon which the oil to be tested is placed. If the oil of
almonds or olives contains only a small quantity of poppy oil when thus
treated, it is entirely converted into crystallized elaidin, whilst the
poppy oil swims on the top in drops.
* * * * *
COLORING MATTER OF VOLATILE OILS.
BY G.E. SACHSSE.
Public-domain text, read in full here on John Shaqi.
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