If a mixture of equal parts of oxide of manganese and chlorate of potash is placed in a clean Florence flask, with a cork, and pewter, or glass tube attached, great quantities of oxygen are quickly liberated, on the application of the heat of a spirit lamp. Such a retort would cost about fourpence, and if the flask is broken in the operation it can be easily replaced by another, value one penny, as the same cork and tube will generally suit a number of these cheap glass vessels. Corks may always [Page 91] be softened by using either a proper cork squeezer, or by placing them under a piece of board or a flat surface, and rolling and pressing the cork till quite elastic. Whilst fitting the latter into the neck of a flask, it is perhaps safer to hold the thin and fragile vessel in a cloth, so that if the flask breaks the chemical experiment may not be arrested for many days by the severe cutting and wounding of the fingers. After the cork is fitted, it is to be removed from the flask and bored with a cork borer. This useful tool is sold in complete sets to suit all sizes of glass tubes, and the pewter or glass being inserted, the flask and tube will be ready for use, provided the tube is bent to the proper curve. This is easy enough to perform with the pewter, but not quite so easy with the glass tube, which must be held over the flame of a spirit lamp till soft, and then bent very gradually to the proper curve. If a short length of the glass tube is heated, it bends too sharply, and the convexity of the glass is flattened, whilst the internal diameter of the tube is lessened, so that at least three inches in length should be warmed, and the heat must not be continued in one place only, but should be maintained in the direction of the bend, the whole manipulation being conducted without any hurry. (Fig. 96.) [Illustration: Fig. 96. A. The cork squeezer. B. The cork borers. C. The operation of bending the glass tube over the flame of the spirit-lamp. D. The neck of the flask, with cork and tube bent and fitted complete for use.] Having filled a gas jar with oxygen, it may be removed from the pneumatic trough by sliding it into a plate under the surface of the water, and to prevent the stopper being thrust out accidentally from the jar by the upward pressure of the gas, whilst a little compressed, during the act of passing it into the plate, it is advisable to hold the stopper of the jar firmly but gently, so that it cannot slip out of its place. A number of jars of oxygen may be prepared and arranged in plates, all of which of course must contain a little water, and enough to cover the welt of the jar. [Page 92] EXPERIMENTS WITH OXYGEN GAS. This gas was originally discovered by Priestley, in August, 1774, and was first obtained by heating red precipitate--_i.e._, the red oxide of mercury. HgO = Hg + O.