The manufacture of earth colours : $b With thirty-one illustrationsBersch, Josef
Science
The manufacture of earth colours : $b With thirty-one illustrations
Bersch, Josef
Coloring matter; Pigments
A simple test for quality consists in weighing out an exact small
quantity (10 grms.), and heating it to a temperature not exceeding 110°
C., until the weight remains constant. A simple calculation then gives
the amount of uncombined water in the sample. Since the proportion of
such water varies in different parts of one and the same deposit, the
test must be repeated, in order to obtain accurate results, on samples
taken from different points, or, preferably, on a properly prepared
average sample.
Even drying changes the colour of ochre considerably. To ascertain the
behaviour of an ochre on calcination, a large sample is dried at 110°
C. until the weight is constant, and divided up into a number of small
samples weighing, say, 10 grms. each. The samples are then heated to
different temperatures, one to the melting-point of lead, another to
that of zinc, and so on.
The higher the temperature employed, the more will the colour of the
ochre approximate to red; and specimens very rich in ferric oxide will
give bright red colours. Beyond this range, a further increase in
temperature will give violet shades, varying with the temperature and
the duration of heating. After this preliminary test, it is desirable
to make another on a larger scale, with quantities up to about 1 lb.
For this test, the different kinds of ochre frequently found in the
same deposit should be mixed together, in order to obtain an idea of
what the mean product, obtained in working on the large scale, will be
like.
On the whole, the results of this second test will be the same as in
the first series, the only object of the second test being to gain
information which may be particularly valuable in practical work. The
bottles in which the calcined samples are stored should be marked with
the temperature and length of heating, so that, when it is subsequently
desired to obtain an ochre corresponding to a particular sample, all
that is necessary will be to heat it to the same degree from the same
length of time. The performance of this simple test will be of great
assistance in standardising the work with a minimum loss of time.
When it is desired to ascertain the composition of an ochre
superficially its behaviour towards hydrochloric acid may be noted. A
weighed quantity of the freshly dug (undried) ochre is treated with
pure acid, free from iron, which will dissolve out the ferric oxide
and lime, leaving clay and quartz sand behind. The presence of lime is
indicated by effervescence on contact with the acid; and if there is no
effervescence, lime is absent. At the end of several hours the acid is
carefully decanted from the undissolved residue which is then stirred
up with water, left to subside, and weighed when dry. This method will
give the amount of substances, other than ferric oxide and lime, in
the sample. These substances usually consist of clay or sand.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account