The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigmentsBersch, Josef
Science
The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigments
Bersch, Josef
Dyes and dyeing; Pigments
When rosin is the raw material, the combustion can be conducted in flat
spoon-shaped vessels placed before a narrow opening into the flue. Fig.
30 shows an arrangement very successful in practice. The spoon-shaped
iron vessel, G, stands in a second, G₁, which is filled with water:
this prevents the fused rosin from becoming too hot. If the temperature
in G rose too high, dry distillation would take place along with the
combustion of the rosin, and the soot would be largely contaminated
by the products of this distillation. This may proceed so far that in
place of the fine flocks of soot a greasy mass is deposited in the
flues, consisting of a mixture of soot with products of distillation,
from which the soot could be obtained only with great difficulty. The
soot and gaseous products of combustion pass through the opening, O,
into the flues, R R. This opening is only several centimetres wide,
but is nearly as long as the combustion vessel. Above the vessel,
G, is a movable iron cover, D, in which are slides by which the air
supply is regulated. The cover is only taken off when fresh material is
introduced.
The air supply cannot be sufficiently regulated by the slides in the
cover; these must be used in conjunction with the chimney damper. The
combustion is observed through a thick glass plate let into the cover.
At the commencement of the operation slides and damper are completely
opened. When the chimney is seen to emit a thick black smoke the flues
are filled with the products of combustion, and the speed with which
they pass through the flues must be regulated. The current of air is
decreased until only a little visible smoke escapes from the chimney,
and the flame is no longer white, but a murky red. It should be noted
that the first soot obtained from a new works is never of the best
quality, the production of this is only gradually attained. The cause
of this is that the new masonry is damp and gives up water to the hot
gases, so that they are cooled and their velocity disturbed; the soot
will also be damp. Thus a greasy soot is obtained. It is of very little
use to allow the installation to remain unused for some months after it
is completed; the brickwork would only dry superficially, and when it
was first heated the presence of the water would become evident.
In order to dry the whole erection to such an extent that the moisture
from the brickwork has no effect on the regular course of the
operation, it is advisable to commence with materials of little value
and to allow a portion of them to be lost by the use of a stronger
draught than is generally used, so that the flues can be freed from
all moisture as soon as possible. This applies equally to all kinds of
arrangements for this purpose.
[Illustration: FIG. 31.]
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