The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigmentsBersch, Josef
Science
The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigments
Bersch, Josef
Dyes and dyeing; Pigments
The soot is ignited in sheet-iron boxes with a coating to protect the
metal from burning. This coating is best made from clay and hair. A
very thin paste of clay and water is painted uniformly over the boxes
with a brush; when the first coat is dry a second and third are given.
When once the metal is completely covered with clay, several coats
are given of clay mixed with chopped tow until the layer is several
millimetres thick. The coating carefully made in this manner is very
durable, and the boxes can be used for a long time, whilst without
the coating they would very soon be burnt. Particular care must be
given to the manufacture of the boxes themselves; the bottoms must fit
very accurately, and should be coated with clay in order to ensure an
air-tight joint. The lids also must fit accurately, and when they are
closed must equally be made tight by clay.
The soot is at first loosely packed into the box and each portion then
pressed with a rammer so that it tightly fills the boxes. In the lid is
a very small opening, through which the volatile products can escape.
The heating begins quite gently at the back, and proceeds gradually to
the front; the boxes are finally brought to a good red heat, at which
they are maintained for about half an hour; at this temperature the
substances mixed with the carbon are almost entirely volatilised, and
the soot acquires its true black appearance. The soot itself attains
a red heat in the boxes and in consequence of its loose nature it
very readily burns. The precautions given above must be observed in
order to protect completely the soot against the action of the air. The
boxes should not have the smallest opening besides that in the cover
necessary for the escape of the volatile matters; through an opening
invisible to the naked eye so much oxygen may enter during the cooling
of the boxes that a considerable quantity of carbon will burn to
carbonic acid.
To avoid losses through the carbon burning precautions must equally be
taken in the cooling of the boxes. When the ignition is finished they
are drawn out of the furnace by tongs and placed upright on a stone
floor; as the cool air enters, and in contact with the red-hot carbon
would burn a portion of it. This can be prevented by a simple artifice:
a red-hot coal is placed on the small opening in the lid; this converts
the oxygen of the air which enters the boxes into carbonic acid. When
all the boxes are taken out of the furnace the doors of the room in
which they are placed are opened, so that they are cooled in the
draught. Finely divided carbon takes fire at a temperature far below a
red heat, so that the boxes should not be opened until their contents
are quite cold. If they were opened whilst hot the soot might take fire.
Public-domain text, read in full here on John Shaqi.
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