The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigmentsBersch, Josef
Science
The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigments
Bersch, Josef
Dyes and dyeing; Pigments
The extractors consist of wooden or copper vessels, slightly conical
in shape, and of sufficient strength to resist the pressure of one
atmosphere. On the top is a copper dome closed by a lid, through which
the raw material is introduced, and also steam and water. Immediately
above the bottom is an opening, also closed by a screw, which serves
to remove the exhausted materials. An inclined sieve is placed at some
distance above the bottom; upon this the material rests. The extract
collects below the sieve, and may be run off by the pipe or brought
into another extractor. All the metallic portions of the apparatus
which come in contact with the liquid must be made of a metal such as
copper, which does not act upon tannic acid. Iron cannot be used; it
forms deep bluish or greenish black compounds with tannic acid, which
would cause the extract, instead of being pale and clear, to resemble
ordinary writing ink.
In a range of 10 extractors the process is carried out in the following
manner: The extractors numbered 1 to 10 are filled with bark or
dye-wood and closed; 1 is then filled with water from the tank, and
heated by steam to 50° to 70° C. After some time the contents of 1 are
forced into 2, and 1 is again filled with water, so that the material
in 2 is in contact with the solution from 1, whilst the material in 1
is warmed with a fresh quantity of water under pressure; the extract
in 2 is transferred to 3, that in 1 to 2, and 1 is again filled with
water, and so on. Finally from 10 a very strong extract of tannin
or colouring matter is obtained. The quantity of water required to
fill one extractor has come ten times in contact with fresh bark
or dye-wood. The material in 1 has been treated with ten times the
quantity of water; it is now exhausted, and is replaced by fresh
material. The sequence of the vessels is now changed. The original
extractor 2 is to be regarded as 1, and 1 as 10. After ten repetitions
the original order of the extractors re-obtains. Ninety-nine per cent.
of the tannic acid of bark is extracted in this way.
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