The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigmentsBersch, Josef
Science
The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigments
Bersch, Josef
Dyes and dyeing; Pigments
_Soft White Lead._—The hard white lead prepared as just described
consists of very heavy and very hard lumps of the purest white. When
soft white lead is required, the admixed lead acetate must be removed
by washing. This is accomplished by adding a larger quantity of water,
either when grinding under the edge-runners or in the mills, so that
a thin pulp is formed; this is run into a receiver, in which is a
stirrer. The white lead is not completely prevented from sinking by the
stirrer; a soft mud is deposited at the bottom of the vessel, which
can only be stirred up with difficulty on account of its high density.
When this vessel is full, the stirrer is stopped and the milky liquid
allowed to settle, which happens in a short time on account of the
high specific gravity of white lead. The clear liquid above the white
lead is drawn off into a tank lined with cement. It is advisable to
arrange the stirrer so that it may be placed at any height in the
vessel; if this is the case, by gradually lowering the stirrer whilst
in motion, the white lead lying at the bottom can be mixed up with
fresh water. These operations are repeated until all the lead acetate
is removed.
Soda solution is added to the wash waters in order to recover the lead
dissolved in them as lead acetate; lead carbonate is precipitated and
settles at the bottom of the tank. This precipitation may also be
effected by putting lumps of limestone in the tank. The paste remaining
in the washing tubs, which now contains only pure white lead and water,
is filled into bags of closely woven material and the water pressed out
by a gradually increasing pressure, until a stiff pulp remains behind.
This is then completely dried, either in the air or in drying stoves.
Soft white lead forms either irregular lumps or a soft, heavy powder.
The lower qualities of white lead contain a smaller or larger quantity
of finely ground barytes; the higher the proportion of barytes the
smaller is the covering power of the mixture. A very simple method for
detecting barytes in white lead will be given later.
(b) GERMAN PROCESS.
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