The Manufacture of Paper: With Illustrations, and a Bibliography of Works Relating to Cellulose and Paper-MakingSindall, R. W. (Robert Walter)
History
The Manufacture of Paper: With Illustrations, and a Bibliography of Works Relating to Cellulose and Paper-Making
Sindall, R. W. (Robert Walter)
Papermaking
_Condition of Sample._--A record should be made of the general
appearance of the sample, its condition and the amount available for
the investigation. Any information available as to the source of supply
and the growth of the plant should also be noted.
_Preparation of Sample._--The material is cut up into small pieces. The
most convenient appliance for this purpose is a mitre cutter as used by
picture-frame makers. If the sample is a piece of wood, sections one
inch thick cut across the grain of the wood are most suitable, as they
can be readily cut up into thin flakes by this machine.
_Moisture in Sample._--A small average sample should be dried at 100°
C. for the determination of moisture.
_Treatment with Caustic Soda._--About two hundred grams of the raw
material is closely packed into a small digester or autoclave and
covered with a solution of caustic soda having a specific gravity of
1·050. A perforated lead disc should be placed above the sample in the
digester to prevent any of it from floating above the level of the
solution. The material should be digested for five or six hours at a
pressure of 50 lbs. The conditions of treatment here given will need to
be varied according to the nature of the fibre. Some materials can be
readily converted into pulp with weaker liquor and at a lower pressure,
while others will require prolonged treatment. These conditions must be
varied according to judgment or according to the effects produced by
the conditions already set out.
_Unbleached Pulp._--The contents of the digester are emptied out into
an ordinary circular sieve provided with a fine copper wire bottom,
having a mesh of about sixteen to the inch. The sieve is immersed in
water and the contents partially washed with hot water. The partially
washed material is squeezed out by hand and tied up in a strong cloth
and then kneaded thoroughly by hand in a basin of water which is
repeatedly renewed until the fibre is thoroughly washed. The process of
kneading at the same time reduces the fibre to the condition of pulp.
The water is carefully squeezed out of the pulp by hand, and the moist
pulp is then divided into two equal parts, the first of which is made
up into sheets of any convenient size, care being taken that none of
the fibre is lost. These sheets are then dried in the air and preserved
as samples of unbleached pulp, a record being made of the weight
produced.
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