The Principles of Chemistry, Volume IMendeleyev, Dmitry Ivanovich
Science
The Principles of Chemistry, Volume I
Mendeleyev, Dmitry Ivanovich
Argon; Chemistry; Periodic law
The pneumatic trough may naturally be made of any material
(china, earthenware, or metal, &c.), but usually a glass one,
as shown in the drawing, is used, as it allows the progress
of the experiment to be better observed. For this reason, as
well as the ease with which they are kept clean, and from the
fact also that glass is not acted on by many substances which
affect other materials (for instance, metals), glass vessels
of all kinds--such as retorts, test tubes, cylinders, beakers,
flasks, globes, &c.--are preferred to any other for chemical
experiments. Glass vessels may be heated without any danger if
the following precautions be observed: 1st, they should be made
of thin glass, as otherwise they are liable to crack from the bad
heat-conducting power of glass; 2nd, they should be surrounded
by a liquid or with sand (Fig. 2), or sand bath as it is called;
or else should stand in a current of hot gases without touching
the fuel from which they proceed, or in the flame of a smokeless
lamp. A common candle or lamp forms a deposit of soot on a
cold object placed in their flames. The soot interferes with
the transmission of heat, and so a glass vessel when covered
with soot often cracks. And for this reason spirit lamps, which
burn with a smokeless flame, or gas burners of a peculiar
construction, are used. In the Bunsen burner the gas is mixed
with air, and burns with a non-luminous and smokeless flame.
On the other hand, if an ordinary lamp (petroleum or benzine)
does not smoke it may be used for heating a glass vessel without
danger, provided the glass is placed well above the flame in the
current of hot gases. In all cases, the heating should be begun
very carefully by raising the temperature by degrees.
[20] In order to avoid the necessity of holding the cylinder, its open
end is widened (and also ground so that it may be closely covered
with a ground-glass plate when necessary), and placed on a stand
below the level of the water in the bath. This stand is called
'the bridge.' It has several circular openings cut through it,
and the gas delivery tube is placed under one of these, and the
cylinder for collecting the gas over it.
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