The Principles of Leather ManufactureProcter, H. R. (Henry Richardson)
History
The Principles of Leather Manufacture
Procter, H. R. (Henry Richardson)
Leather
As soon as the contents of the basins appear completely dry, they may be
transferred to the drying oven. The most satisfactory form is one in
which the basins are placed in a closed chamber, surrounded by steam at
the atmospheric pressure, and at the same time subjected to a vacuum
maintained by a water-jet air-pump; but as this apparatus is somewhat
costly, it will probably only be provided in laboratories which make a
speciality of such work. Next to the vacuum-oven, an air-oven, heated by
a gas-burner, and with its temperature controlled by a mercurial
regulator to 100-105° C., gives the best results, and it is also the
cheapest; but considerable care and some scientific knowledge are
required to work it satisfactorily. In intelligent hands good results
may be got from the small “breakfast cooker” gas ovens made by Fletcher
of Warrington, which are placed on an iron plate heated by a gas burner,
the supply of gas to which is regulated by a thermostat, or mercurial
gas-regulator, inserted, together with a thermometer, through holes
drilled in the top. The basins must not be placed too near the bottom of
the oven, which must be protected by a perforated metal plate supported
perhaps one inch above it, to prevent radiation and to distribute the
hot air. Any cold air required for ventilation should be admitted below
this plate, and care should be taken to exclude the products of the
burning gas. Contact of the basins with any heated part of the
metal-work should be carefully avoided, and they are best supported on
grid-shelves covered with wire gauze or perforated metal, so as to allow
of free circulation of air. If perforated zinc is used, it must be well
supported, as it is much softened at the temperature used. The least
satisfactory appliance in skilled hands, but probably the most easy to
work by the inexperienced, is the ordinary water- or steam-oven. It is
impossible, in this apparatus, to raise the temperature of the interior
fully to boiling point, and below this gambier, quebracho, and other
solutions containing catechins (p. 298), dry very slowly. On the other
hand, so long as it is kept boiling and supplied with water, the
temperature is necessarily constant, and there is no danger of
overheating, which easily occurs in ovens heated directly by gas. Such
ovens are often fitted with openings at the top for use as a steam-bath.
To get the best results, the basins must be as freely exposed as
possible to the air in the interior of the oven (in no case must basins
be set one inside another, except in the exsiccator for cooling), and
little or no ventilation from the outside is required, as only traces of
moisture remain after evaporation on the steam-bath; so that, after an
hour’s drying, any ventilators may safely be closed. As a good deal of
cooling takes place through the door, it is best to protect it with some
non-conducting material, such as asbestos millboard, which may be
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