The Principles of Leather ManufactureProcter, H. R. (Henry Richardson)
History
The Principles of Leather Manufacture
Procter, H. R. (Henry Richardson)
Leather
attached with rivets, or even with ordinary paper-fasteners. One to one
and a half hours will be required to dry to constance in the
vacuum-oven; two to three in the air-oven at 105°; and probably about
four hours in the water-oven, except in the case of gambiers, which may
require somewhat longer. Too long heating is disadvantageous, as the
residues begin to oxidise and gain in weight. As soon as it is judged
that the basins will be constant in weight, they are withdrawn from the
drying oven, and at once placed in an exsiccator (a glass vessel with an
accurately fitted lid, which should be slightly greased, in the bottom
part of which is placed either dry calcium chloride or concentrated
sulphuric acid, to absorb the moisture of the air it contains). In this
they are left till thoroughly cold, which if several basins are put in
together, may require half an hour. They are then weighed accurately,
but as rapidly as possible; returned to the drying oven for half an
hour; and replaced in the exsiccator. The exact weight of each basin, as
it comes in turn to be weighed, is now placed on the balance before
removing the basin from the exsiccator, so that it can be seen instantly
if there is loss or gain of weight, before it has time to absorb any
moisture from the air. The weight should not be more than a milligram or
so less than at the first weighing; if weight has been gained, it is
caused by oxidation, and the first weight should be taken as correct if
it is certain that the basin was then perfectly cold; a very slight
amount of warmth easily reducing the apparent weight by several
milligrams. If material loss has occurred, the basin must of course be
returned to the oven, and re-weighed in another half hour; but with
experience, this should rarely be needed.
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