10. A portion evaporated on the sandbath rather hastily, gave a dry saline mass, quite unlike that left by the _saturated solution_ already described (6); and which, when dissolved, had the same astringent taste as before, and bleached solution of indigo very powerfully: when compared with an equal portion of the unevaporated solution, which had been placed in the mean time in the dark, its bleaching power upon diluted sulphate of indigo was 30, that of the former being 76. Another portion, evaporated in a still more careful manner, gave a mass of damp crystals, which, when dissolved, had the taste, smell, and bleaching power of the original solution, with almost equal strength. 11. These experiments shewed sufficiently that the whole of the chlorine had not acted upon the carbonate of soda to produce chloride of sodium, and chlorate of soda; that much was in a peculiar state of solution or union which enabled it to withstand ebullition, and yet to act freely as a bleaching or disinfecting agent; and that probably little or none had combined with the sodium, or been converted into chloric acid. To put these ideas to the test, two equal portions of the Labarraque solution were taken; one was put into a large tube, closed at one extremity, diluted sulphuric acid was added till in excess, and then air blown through the mixture by a long small open tube, proceeding from the mouth, for the purpose of carrying off the chlorine; the contents of the tube were then heated nearly to the boiling point, air being continually passed through. In this way all the chlorine which had combined with the carbonated alkali without decomposing it, was set free by the sulphuric acid, and carried off by the current of air and vapour, whilst any which had acted chemically upon the alkali would, [p088] after the action of the sulphuric acid, be contained in solution as muriatic and chloric acids, and from the diluted state of the whole, would not be removed by the after-process, but remain to be rendered evident by tests. The other portion being diluted, had sulphuric acid added also in excess, but no attempt was made to remove the chlorine. Equal quantities of these two portions in the same state of dilution were then examined by nitrate of silver for the quantities of chlorine sensible in them, and it was found that the latter portion, or that which retained the whole of the chlorine thrown into it, contained above sixty times as much as the former.