The Romance of the Microscope: An interesting description of its uses in all branches of science, industry, agriculture, and in the detection of crime, with a short account of its origin, history, and developmentEaland, C. A. (Charles Aubrey)
History
The Romance of the Microscope: An interesting description of its uses in all branches of science, industry, agriculture, and in the detection of crime, with a short account of its origin, history, and development
Ealand, C. A. (Charles Aubrey)
Microscopes; Microscopy
Some strikingly beautiful results may be obtained in another manner;
the method is used by analysts in their so-called fusion tests. We
take a small grain of some substance, say, lead nitrate, place it in
the centre of our slide, cover with a cover slip, and warm over a
flame till it melts. Then, taking a similar-sized grain of another
substance, such as saltpetre, we place it against the edge of the cover
slip on the side opposite to the lead nitrate. Further warming will
cause the saltpetre to melt, and run below the slide and mix with the
lead nitrate. If we watch the meeting of the two chemicals a wonderful
sight will reward us. The lead compound forms a “beautiful crystalline
skeleton,” whilst the saltpetre forms six-sided stars at the opposite
side of the cover slip. The experiment may be repeated, using lunar
caustic and saltpetre, also the iodides of silver and potassium; in
fact we may try any chemical substances we have at hand, though we
shall find that some do not melt very easily, and potassium chlorate
is somewhat dangerous, for it forms explosive compounds with certain
substances.
The number of interesting and beautiful objects which may be obtained
by so-called solution tests is practically unlimited, and the
enthusiastic microscopist will certainly try all the tests we describe
as well as many others of his own invention. Should the chemist wish to
detect the presence of aluminium in very small quantities, he relies on
his microscope and proceeds in the following manner. He takes a drop of
the solution, suspected of containing alum, and adds to it a drop of
sulphuric acid. This mixture he puts on his slide, which he heats over
a flame till dry. Now he adds a drop of water, and then a very small
amount of calcium chloride is brought to the edge of the water. Beneath
his microscope he can now watch the formation of beautiful colourless,
eight-sided crystals which denote the presence of aluminium.
Public-domain text, read in full here on John Shaqi.
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