The Sceptical Chymist: or Chymico-Physical Doubts & Paradoxes, Touching the Spagyrist's Principles Commonly call'd Hypostatical; As they are wont to be Propos'd and Defended by the Generality of Alchymists. Whereunto is præmis'd Part of another Discourse relating to the same Subject.Boyle, Robert
Philosophy
The Sceptical Chymist: or Chymico-Physical Doubts & Paradoxes, Touching the Spagyrist's Principles Commonly call'd Hypostatical; As they are wont to be Propos'd and Defended by the Generality of Alchymists. Whereunto is præmis'd Part of another Discourse relating to the same Subject.
Boyle, Robert
Chemistry -- Early works to 1800
Proceed we then in the next place to consider, That there are divers
Separations to be made by other means, which either cannot at all, or
else cannot so well be made by the Fire alone. When Gold and Silver
are melted into one Mass, it would lay a great Obligation upon
Refiners and Goldsmiths to teach them the Art of separating them by
the Fire, without the trouble and charge they are fain to be at to
sever them. Whereas they may be very easily parted by the Affusion of
Spirit of Nitre or _Aqua fortis_ (which the French therefore call _Eau
de Depart_:) so likewise the Metalline part of Vitriol will not be so
easily and conveniently separated from the Saline part even by a
violent Fire, as by the Affusion of certain Alkalizate Salts in a
liquid Form upon the Solution of Vitriol made in common water. For
thereby the acid Salt of the Vitriol, leaving the Copper it had
corroded to joyn with the added Salts, the Metalline part will be
precipitated to the bottom almost like Mud. And that I may not give
Instances only in De-compound Bodies, I will add a not useless one of
another kinde. Not only Chymists have not been able (for ought is
vulgarly known) by Fire alone to separate true Sulphur from Antimony;
but though you may finde in their Books many plausible Processes of
Extracting it, yet he that shall make as many fruitlesse Tryals as I
have done to obtain it by, most of them will, I suppose, be easily
perswaded, that the Productions of such Processes are Antimonial
Sulphurs rather in Name than Nature. But though Antimony sublim'd by
its self is reduc'd but to a volatile Powder, or Antimonial Flowers,
of a compounded Nature like the Mineral that affords them: yet I
remember that some years ago I sublim'd out of Antimony a Sulphur, and
that in greater plenty then ever I saw obtain'd from that Mineral, by
a Method which I shall therefore acquaint you with, because Chymists
seem not to have taken notice of what Importance such Experiments may
be in the Indagation of the Nature, and especially of the Number of
the Elements. Having then purposely for Tryals sake digested eight
Ounces of good and well powder'd Antimony with twelve Ounces of Oyl of
Vitriol in a well stopt Glas-Vessel for about six or seven Weeks; and
having caus'd the Mass (grown hard and brittle) to be distill'd in a
Retort plac'd in Sand, with a strong Fire; we found the Antimony to be
so opened, or alter'd by the _Menstruum_ wherewith it had been
digested, That whereas crude Antimony, forc'd up by the Fire, arises
only in Flowers, our Antimony thus handled afforded us partly in the
Receiver, and partly in the Neck and at the Top of the Retort, about
an Ounce of Sulphur, yellow and brittle like common Brimstone, and of
so Sulphureous a smell, that upon the unluting the Vessels it infected
the Room with a scarce supportable stink. And this Sulphur, besides
the Colour and Smell, had the perfect Inflamability of common
Brimstone, and would immediately kindle (at the Flame of a Candle) and
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