Liecke in Dingler’s Polytechnical Journal, prescribes the following
formulæ for manufacturing the three several preparations,
Mono-Nitro-Glycerin, Di-Nitro-Glycerin and Tri-Nitro-Glycerin.
Mono-Nitro-Glycerin:
Glycerin 100 grammes.
Nitric acid, Sp. Gr. 1.3, 200 grammes.
Dissolve the Glycerin in the nitric acid, and then add
sulphuric acid 200 cubic centimeters.
The product should be C³H⁵O²H}
}O⁴
NO⁴H}
Di-Nitro-Glycerin:
Sulphuric acid containing 1 eq. water, two volumes,
nitric acid, Sp. Gr. 1.4, one volume; mix the above,
lower the temperature to 32°F, or below, and drop into it
Glycerin, pure, one volume.
Prod. C³H⁵O²H}
}O⁴
2NO⁴}
Tri-nitro-glycerin:
Sulphuric Acid, 3.5 parts.
Nitrate of Potash, 1 part.
cooled to 0°F, produces KO + 4SO³ + 6HO, from this the
concentrated fuming Nitric acid is separated by decantation,
and being maintained at 0°F,
Glycerin 0.8 parts is very gradually added,
producing C³H⁵O²NO⁴}
}O⁴
2NO⁴}
From the above extracts of several of the most eminent chemists of
the present day, the reader will glean, that in order to prepare this
explosive, of uniform quality, invariable in composition, free from
water, or any other impurity, it is not merely necessary to buy the
best materials, but to have at command the means of verifying their
purity before attempting its manufacture.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account