of one hundred and sixteen stone pitchers which are arranged in nine
wooden troughs placed in the centre and at the end of the room, and
these troughs are now filled with ice-cold water, or ice and salt, so
as to rise within four inches of the top of the jar. On shelves above
the troughs, are arranged glass jars, one to each stone pitcher. Into
each of these glass jars, two pounds, by weight, of pure Glycerin is
poured, and this, by means of a siphon, with a rubber tube attached,
about two feet long, falls drop by drop into the corresponding pitcher
of mixed sulphuric and nitric acids. Immediately below the shelf, in
which the Glycerin jar stands, is a 2¼ inch iron pipe, which brings a
current of cold air from the receivers connected with the two blowers
before-mentioned. This current of air is distributed to each jar,
while the acid and glycerin are mixing, by a rubber pipe, to which is
attached a glass tube 16 inches long, and with a ¼ inch bore. During
the hour and a half to two hours that the glycerin takes to run off
into the pitchers, the greatest care, and the closest attention is
requisite. The three men whose duty it is to attend to the mixing
process, have each a row of pitchers to watch, walking the whole
time up and down, beside them, with thermometer in hand, and as the
nitrous fumes rise from the forming Nitro-Glycerin, they stir the
mixture, with the glass tube before-mentioned, in any pitcher that
may be giving out too violent fumes. Sometimes this is caused by the
glycerin running a little freely, which fires the mixture, wastes the
glycerin, forming oxalic acid, and developes unpleasant vapors. In
such a case, by pushing back a little wooden peg in the glass jar, the
flow of glycerin is lessened, and by stirring with the glass tube the
nitrous vapors dispelled. Should the engine also stop working by any
unforseen circumstance, the current of air will of course be stopped,
when the mixture will take fire. In this case, it is necessary to
stir the mixture, and at once stop the flow of glycerin. When the
glycerin and acid is all mixed, and the nitrous fumes cease to appear,
the Nitro-Glycerin from each pitcher is dumped into a large tank of
water, at a temperature of 70°, about 450 lbs. of Nitro-Glycerin being
the amount of each batch manufactured. The Nitro-Glycerin sinks
to the bottom and is covered by about six feet of water. Here it
remains for fifteen minutes to be subsequently washed free from any
impurities. This tank goes through the floor into a basement chamber,
its bottom being on a slight incline, so that the Nitro-Glycerin may
run out easily. The water is first drawn off from the top of the
Nitro-Glycerin, and then the latter is run into a wooden swinging tub,
in shape somewhat like an old-fashioned butter churn, but a good deal
larger in diameter. In this it is washed five times, three times with
plain water, and twice with soda, a current of air working through it
at the same time.
Public-domain text, read in full here on John Shaqi.
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