A handbook of laboratory glass-blowingBolas, Bernard D. (Bernard Dell)
Science
A handbook of laboratory glass-blowing
Bolas, Bernard D. (Bernard Dell)
Glass blowing and working
We now need to make three projections of glass rod. These are produced
as follows:--Heat the end of the glass rod until a thoroughly melted
mass of glass has accumulated (the rod must be rotated while this is
being done, otherwise the glass will drop off); when sufficient melted
glass has been obtained, the edge of the turned-out foot should be
heated to dull redness over about one-third of its circumference, and
the melted glass on the rod should be drawn along the heated portion
until both are so completely in contact as to form one mass of
semi-fluid glass. The rod should now be drawn away slowly, and, finally,
separated by melting off, thus producing a flat projection. A repetition
of the process will give the other two projections, and the finished
foot may be adjusted to stand upright by heating the projections
slightly and standing it on the carbon plate mentioned on page 7. After
the foot is adjusted it should be annealed slightly by heating to just
below the softening point of the glass and then rotating in a smoky gas
flame until it is covered with a deposit of carbon, after which it
should be allowed to cool in a place free from draughts and where the
hot glass will not come in contact with anything. The finished foot is
shown by _k_, Fig. 7.
_Building up from Glass Rod._--A glass skeleton-work can be constructed
from rod without much difficulty, and is sometimes useful as a container
for a substance which has to be treated with acid, or for similar
purposes. The method is almost sufficiently explained by the
illustration in Fig. 7; _f_ shows the initial stage, _g_ the method of
construction of the net-work, and _h_ the finished container. It is
convenient to introduce the substance at the stage indicated by _g_. The
important points to observe in making this contrivance are that the
glass rod must be kept hot by working while it is actually in the flame,
and that the skeleton must be made as thin as possible with the
avoidance of heavy masses of glass at any place. If these details are
neglected it will be almost certain to crack.
_Stirrers._--These are usually made from glass rod, and no special
instructions are necessary for their construction, except that the glass
should be in a thoroughly fused condition before making any joins and
the finished join should be annealed slightly by covering with a deposit
of soot, as explained on page 16. The flat ends shown in _a_, Fig. 8,
are made by squeezing the soft glass rod between two pieces of carbon,
and should be re-heated to dull redness after shaping. Fig. 8 also shows
various forms of stirrer.
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A handbook of laboratory glass-blowing — John Shaqi
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