A handbook of laboratory glass-blowing — John Shaqi
A handbook of laboratory glass-blowingBolas, Bernard D. (Bernard Dell)
Science
A handbook of laboratory glass-blowing
Bolas, Bernard D. (Bernard Dell)
Glass blowing and working
In order to carry out stirring operations in the presence of a gas or
mixture of gases other than air, some form of gland or seal may be
necessary where the stirrer passes through the bearing in which it runs.
A flask to which is fitted a stirrer and gas seal is shown in section by
_b_, Fig. 8. The liquid used in this seal may be mercury, petroleum, or
any other that the experimental conditions indicate.
[Illustration: Fig. 8]
If the bearing for a stirrer is made of glass tube, it is desirable to
lubricate rather freely; otherwise heat will be produced by the
friction of the stirrer and the tube will probably crack. Such
lubrication may be supplied by turning out the top of the bearing tube
and filling the turned-out portion with petroleum jelly mixed with a
small quantity of finely ground or, better, colloidal graphite, and the
bearing should also be lubricated with the same composition. Care
should be taken not to employ so soft a lubricant or so large an excess
as to cause it to run down the stirrer into the liquid which is being
stirred.
_Leading a Crack._--It sometimes happens that a large bulb or specially
thin-walled tube has to be divided. In such a case it is scarcely
practicable to use the method recommended for small tubes on page 12,
but it is quite easy to lead a crack in any desired direction. A
convenient starting point is a file cut; this is touched with hot glass
until a crack is initiated. A small flame or a bead of hot glass is now
used to heat the article at a point about a quarter of an inch from the
end of the crack and in whatever direction it has to be led. The crack
will now extend towards the source of heat, which should be moved
farther away as the crack advances. In this manner a crack may be caused
to take any desired path and can be led round a large bulb.
_Cutting Glass with the Diamond._--Slips of window-glass can be used in
place of glass rod for some purposes, and as cutting them involves the
use of the glaziers' diamond or a wheel-cutter, they may well be
mentioned under this heading.
In cutting a sheet of glass with the diamond, one needs a flat surface
on which to rest the glass, and a rule against which to guide the
diamond. The diamond should be held in an almost vertical position, and
drawn over the surface of the glass with slight pressure. While this is
being done the angle of the diamond should be changed by bringing the
top of the handle forward until the sound changes from one of scratching
to a clear singing note. When this happens the diamond is cutting. A few
trials will teach the student the correct angle for the diamond with
which he works, and the glass, if properly cut, will break easily. If
the cut fails it is better to turn the glass over and make a
corresponding cut on the other side rather than make any attempt to
improve the original cut. The diamond is seldom used for cutting small
glass tubes.
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