A Practical Handbook on the Distillation of Alcohol from Farm Products — John Shaqi
A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
Supposing, again, that vapors containing but a small quantity of alcohol
are brought into contact with an alcoholic liquid of lower temperature
than the vapors themselves, and in very small quantity, the vapor of
water will be partly condensed, so that the remainder will be richer in
alcohol than it was previously. But the water, in condensing, converts
into vapor a portion of the spirit contained in the liquid interposed, so
that the uncondensed vapors passing away are still further enriched by
this means. Here, then, are the results obtained; the alcoholic vapors
are strengthened, firstly, by the removal of a portion of the water
wherewith they were mixed; and then by the admixture with them of the
vaporized spirit placed in the condenser. By the employment of some such
method as this, a very satisfactory yield of spirit may be obtained, both
with regard to quality, as it is extremely concentrated, and to the cost
of production, since the simple condensation of the water is made use of
to convert the spirit into vapor without the necessity of having recourse
to fuel. The construction of every variety of distilling apparatus now in
use is based upon the above principles.
A sectional view of another simple form of still is shown in Fig. 8; _V_
is a wooden vat having a tight fitting cover _a_, through the center of
which a hole has been cut. The wide end of a goose neck of copper pipe
_g_ is securely fitted over this aperture, the smaller end of this pipe
passes through the cover of the retort _R_ extending nearly to the
bottom; _f_ is the steam supply pipe from boiler; _M_ the rectifier
consisting of a cylindrical copper vessel containing a number of small
vertical pipes surrounded by a cold water jacket; _o_ the inlet for the
cold water which circulates around these small pipes, discharging at _n_;
the pipes in _M_ have a common connection to a pipe _p_, which connects
the rectifier with coil in cooler _C_; _s_ is a pipe to the receptacle
for receiving the distillate; _u_ cold water supply pipe to cooler, and
_W_ discharge for warmed-up water, _k_ discharge for refuse wash in vat
_V_.
[Illustration: FIG. 8.--Simple Still, with Rectifier.]
The operation is as follows: The vat _V_ is nearly filled with fermented
mash and retort _R_ with weak distillate from a previous operation. Steam
is then turned into the pipe _f_ discharging near the bottom of the vat
_V_ and working up through the mash. This heats up the mash and the
vapors escape up _g_ over into _R_ where they warm up the weak
distillate. The vapors thus enriched rise into _M_, where a good
percentage of the water vapor is distilled, that is, condensed by the
cold water surrounding the small pipes. The vapor then passes over
through _p_ into the coil, where it is liquified and from whence it
passes by pipe _s_ into the receiver. The cold water for cooling both _M_
and _C_ can be turned on as soon as the apparatus has become thoroughly
heated up.
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