A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
The process of rectification may be carried on in the apparatus shown in
Figs. 35 and 36. _A_ is a still which contains the spirit to be
rectified; it should be four-fifths full. The condenser _E_ and the
cooler _G_ are filled with water. After closing the cocks _L_ and _I_,
the contents of the still are heated by steam, which is introduced at
first slowly. The vapors of spirit given off pass, by tubes _b_, above
each plate _a_, of the series in column _B_, and escape through _C_ and
_D_ into the condenser _E_, where they are condensed on reaching the
lentils _d d¥_, and return in a liquid state through pipe _f_ and
connections _g g¥_ to the upper plates of the column _B_. In these return
pipes the liquid is volatilized, and constantly recharged with alcohol to
be again condensed, until the water in the condenser is hot enough to
permit the lighter alcoholic vapors to pass into the coil _c c c_,
without being reduced to the liquid state. When this is the case, the
vapors pass through _F_ into the cooler _G_, where they undergo complete
condensation. Great care must be taken that the heat is not so great as
to permit any of the vapors to pass over uncondensed or to flow away in a
hot state; and also to keep up a constant supply of water in the cooler
without producing too low a temperature; the alcoholic products should
run out just cold. The highly volatile constituents of the spirit come
over first, that which follows becoming gradually purer until it consists
of well-flavored alcohol; after this comes a product containing the
essential oils. The more impure products are kept apart from the rest
and re-distilled with the next charge. Some hours generally elapse before
alcohol begins to flow from the cooler. The purest alcohol is obtained
while its strength is kept between 92∞ and 96∞ Baume, and the operation
is complete when the liquid flowing through the vessel marks not more
than 3∞ or 4∞ Baume; it is better, however, to stop the still when the
backing or "faints" indicate 10∞, because the product after this point
contains much fusel-oil, and is not worth collecting.
[Illustration: FIG. 36.--Section of Rectifying Still.]
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