A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
In order to cleanse the apparatus--which should be performed after each
working--the still _A_ is emptied of water by opening the cock _Q_. The
contents of the condenser are then emptied in like manner by opening the
cock _J_, through which they flow upon the plates in the column _B_, and
wash out essential oils which remain in them. These two cocks are then
closed, and the door _U_ in the still head is removed. The water in the
cooler _G_ is then run by means of pipe into the still _A_, so as
partially to cover the steam-coil in the latter. After again securing the
door _U_, a strong heat is applied, and the water in the still is well
boiled, the steam evolved thoroughly cleansing all the different parts of
the apparatus; this is continued for 15 or 20 minutes, when the heat is
withdrawn and the still left to cool gradually.
In the intermittent rectifying still above described the impure products
are distilled with the next charge. In the apparatus as perfected and
used in large distilleries or rectification plants, the division of the
several products composing the phlegm or raw spirit is made at one time
and continuously on the principle now to be described.
It was stated in the beginning of this chapter that the various
impurities in alcohol, the ethers, the water and the fusel oils, have
each their own vaporizing point and each their own condensing point. As
this is so, they may be separated from each other and from the alcohol on
the same principle as we have seen that water is separated from the
mixture of pure alcohol and water; that is, by fractionation, as it is
termed, or by "sifting out" one body from another.
[Illustration: FIG. 37.--Fractional Distilling Apparatus.]
Thus in fractional distillation, each condenser or retort in the
apparatus shown in Fig. 37, above acts as a sieve or trap, letting pass
the most volatile substances but retaining those of a less degree of
volatility. By passing the mixed vapor together through a good condensing
medium the temperature of which is lower than the boiling point of the
less volatile, but not so low as the boiling point of the more volatile
the vapors of the less volatile liquid will be condensed, while the more
volatile will retain their gaseous form. Thus by having a number of
condensing mediums each one slightly lower in temperature than the other,
the various vapors with their various points of volatilization will be
successively condensed, allowing the passage of the more volatile vapors
over to the condenser beyond.
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