A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
In Europe, Gay-Lussac's hydrometer and tables are chiefly used for
alcoholometric testing. This instrument is precisely similar in
construction to those of Twaddle and Baume. On the scale, zero is
obtained by placing it in pure distilled water at 59∞ F., and the highest
mark, or 100, by placing it in pure alcohol at the same temperature, the
intermediate space being divided into 100 equal divisions, each
representing one per cent. of absolute alcohol. The correction for
temperature, as in the above cases, is included in the reference tables.
Another hydrometer, used in France for alcoholometric determinations, is
Cartier's. In form it is precisely similar to Baume's hydrometer. Zero is
the same in both instruments, but the point marked 30∞ in Cartier's is
marked 32∞ in Baume's, the degrees of the latter being thus diminished in
the proportion of 15 or 16. Cartier's hydrometer is only used for liquids
lighter than water.
The alcoholmeter of Tralles is the official instrument for testing
alcoholic liquors in the U. S. but the instrument which is most generally
used both here and abroad is that of BeaumÈ. There are two instruments
bearing BeaumÈ's name, one for liquids lighter than water, the other for
those which are heavier. All hydrometers, alcoholmeters and
saccharometers work on the same principle, though they are each
differently graduated for the particular work to be done and the details
of the measuring process are slightly different. All these instruments
are provided with tables whereby their readings may be corrected and the
specific gravity of the liquid determined.
The above hydrometric methods can be safely employed only when the spirit
tested contains a very small amount of solid matter, since, when such
matter is contained in the liquor in quantity, the density alone cannot
possibly afford a correct indication of its richness in alcohol. Many
methods have been proposed for the estimation of alcohol in liquor,
containing saccharine coloring and extractive matters, either in solution
or suspension. Undoubtedly the most accurate of these, though at the same
time the most tedious, is to subject the liquor to a process of
distillation by which a mixture of pure alcohol and water is obtained as
the distillate. This mixture is carefully tested with the hydrometer, and
the percentage of alcohol in it determined by reference to the tables as
above described; from this quantity and the volume of the original liquor
employed the percentage by volume of alcohol in that liquor is readily
found. The condensing arrangement must be kept perfectly cool, if
possible in a refrigerator, as the alcohol in the distillate is very
liable to be lost by re-evaporation. When great accuracy is desired, and
time is at the operator's disposal, the above method is preferable to all
others.
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