A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
It is performed in the following manner: Three hundred parts of the
liquor to be examined are placed in a small still, or retort, and exactly
one-third of this quantity is distilled over. A graduated glass tube is
used as the receiver, in order that the correct volume may be drawn over
without error. The alcoholic richness of the distillate is then
determined by any of the above methods, and the result is divided by
three, which gives at once the percentage of alcohol in the original
liquor. The strength at proof may be calculated from this in the ordinary
way.
If the liquor be acid, it must be neutralized with carbonate of soda
before being submitted to distillation. From eight to ten per cent. of
common salt must be added, in order to raise the boiling point, so that
the whole of the spirit may pass over before it has reached the required
measure. In the case of the stronger wines it is advisable to distil over
150 parts and divide by two instead of three. If the liquor be stronger
than 25 per cent. by volume of alcohol, or above 52 to 54 per cent.
under-proof, an equal volume of water should be added to the liquid in
the still, and a quantity distilled over equal to that of the sample
tested, when the alcoholic strength of the distillate gives, without
calculation, the correct strength required. If the liquor be stronger
than 48 to 50 per cent. under-proof, three times its volume of water must
be added, and the process must be continued until the volume of the
distillate is twice that of the sample originally taken. In each case the
proportionate quantity of common salt must be added.
For the estimation of alcohol in wines, liquors, etc., the following
method may be employed: A measuring flask is filled up to a mark on its
neck with the liquor under examination, which is then transferred to a
retort; the flask must be carefully rinsed out with distilled water, and
the rinsings added to the liquor in the retort. About two-thirds are then
drawn over into the same measuring flask, and made up to its previous
bulk with distilled water, at the same temperature as that of the sample
before distillation. The strength is then determined by means of Syke's
hydrometer, and this, if under-proof, deducted from 100, gives the true
percentage of proof-spirit in the wine.
[Illustration: FIG. 53.--Field's Alcoholometer.]
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